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1、DataFileC:LCMSDATA2011-06-272011-04-142011-06-2717-28-03ACN-LLY-00002-70A.DSampleName:ACN-LLY-00002-70A=====================================================================Acq.Operator:AcornPharmaTechSeq.Line:4Acq.Instrument:Instrument1Location:Vial10InjectionDate:6/27/20116:06:56PMInj:1InjVolum

2、e:5.000µlDifferentInjVolumefromSequence!ActualInjVolume:1.000µlAcq.Method:C:LCMSDATA2011-06-272011-04-142011-06-2717-28-0320-8010MIN25CM+.MLastchanged:4/18/20112:30:11PMbygongbinAnalysisMethod:C:CHEM321METHODSDEF_LC.MLastchanged:6/28/20119:05:16AMbyAcornPharmaTech(modifiedafterloading)Additi

3、onalInfo:Peak(s)manuallyintegratedDAD1A,Sig=254,4Ref=off(C:LCMSDATA2011-06-272011-04-142011-06-2717-28-03ACN-LLY-00002-70A.D)mAU84.5120031000800600400200576601.0.3.701240123456789minMSD1TIC,MSFile(C:LCMSDATA2011-06-272011-04-142011-06-2717-28-03ACN-LLY-00002-70A.D)ES-API,Pos,Scan,F281600000.

4、53140000012000001000000888000004.367983460469.790668.282858.8.7112748.6.8.1.5600000156210948929726.2.6.87.188996782943883.5.9.3.6.87784000002079.3.8.0.2.3444555.8.0.2.3223320000001110123456789minInstrument16/28/20119:06:08AMAcornPharmaTechPage1of12DataFileC:LCMSDATA2011-06-272011-04-142011-06-271

5、7-28-03ACN-LLY-00002-70A.DSampleName:ACN-LLY-00002-70AMSSignal:MSD1TIC,MSFile,ES-API,Pos,Scan,Frag:80Spectraaveragedoverupperhalfofpeaks.NoiseCutoff:1000counts.ReportableIonAbundance:>10%.RetentionMol.WeightTime(MS)MSAreaorIon0.82668674359.25I219.10I192.10I187.20I141.10I121.15I115.10I112.10I110.10I

6、102.20I84.10I80.20I1.007112293359.25I219.10I187.10I141.10I115.10I110.10I102.10I84.15I80.10I1.27879796359.25I261.20I239.20I219.15I192.15I187.10I141.10I121.15I115.10I112.10I110.10I102.20I84.15I80.10I1.392115243359.30I329.20I319.20I219.15I192.05I187.10I141.10I121.20I115.10I112.10IInstrument16/28/20119:

7、06:08AMAcornPharmaTechPage2of12DataFileC:LCMSDATA2011-06-272011-04-142011-06-2717-28-03ACN-LLY-00002-70A.DSampleName:ACN-LLY-00002-70A111.05I110.10I102.10I84.15I80.10I1.8641925944303.15I298.20I297