仪器分析化学实验

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1、时间就是金钱，效率就是生命！目录仪器分析化学实验大学化学实验化学工艺学实验唯有惜时才能成功，唯有努力方可成就！时间就是金钱，效率就是生命！目录实验1气相色谱法分析混合样品中苯、甲苯和二甲苯··············001实验2醇系物的气相色谱分析·································009实验3烷烃类混合物的定性、定量分析··························012实验4邻二甲苯中杂质的气相色谱分析·························015实验5乙酸正丁酯中杂质的气相色谱分析—内标法定量···········020实验6高效

2、液相色谱法测定车前子和车前草中苯乙醇苷化合物·····025实验7高效液相色谱法定量分析肉苁蓉中的苯乙醇苷化合物·······032实验8高效液相色谱法检测食品中苏丹红Ⅰ染料·················035实验9反相HPLC分析茶叶中的咖啡因···························039实验10pH玻璃电极响应斜率及溶液pH的测定·····················043实验11氯离子选择性电极性能的测试···························047实验12氟离子选择性电极测定自来水中的微量氟·················051实验13

3、循环伏安法测定电极反应参数···························055实验14阳极溶出伏安法测定水中微量镉························059实验15电化学循环伏安技术和电位阶跃技术研究金属电结晶······063实验16稳定恒电位法测定铁钝化阳极极化曲线···················068实验17硫酸铜电解溶液中氯离子的电位测定·····················073唯有惜时才能成功，唯有努力方可成就！时间就是金钱，效率就是生命！实验18弱电解质的电离常数的测定·····························076实验1

4、9火焰原子吸收法灵敏度和水样中铜含量的测定·············080实验20火焰原子吸收光谱法测定土壤中的铜（标准加入法）·········084实验21原子吸收光谱法测定水中镁的含量·······················088实验22原子吸收光谱法测定毛发中的锌·························092实验23火焰原子吸收光谱法测定豆乳粉中微量元素···············096实验24原子发射光谱定性分析·································099实验25微波等离子体炬原子发射光谱定量测定Cd含量···········

5、·107实验26铬天青S分光光度法测定微量铝（铝的二元、三元络合物的比较）··························································111实验27甲基橙解离常数的测定·································114实验28紫外吸收光谱的测定及溶剂性质对吸收光谱的影响·········117实验29蒽醌的紫外吸收光谱法测定·····························121实验30示差分光光度法测定铬·································124实验31紫外分光光度

6、法测定混合物中非那西汀和咖啡因的含量·····128实验32络合物的组成和不稳定常数的测定·······················131实验33聚苯乙烯薄膜红外光谱的测定···························135实验34苯甲酸的红外光谱的测定—KBr压片法制样················141实验35用IR法区分顺、反丁烯二酸······························145实验36荧光素含量的测定·····································148实验37氨基酸的荧光激发、发射及同步荧光光谱的测量······

7、······152实验38荧光光度法测定维生素B2·······························155唯有惜时才能成功，唯有努力方可成就！时间就是金钱，效率就是生命！仪器分析化学实验主编：毕淑云刘春明副主编：田利王强吉林大学出版社前言唯有惜时才能成功，唯有努力方可成就！时间就是金钱，效率就是生命！分析化学实验是化学及相关专业学生必修的一门主干课，而仪器分析化学实验是分析化学实验课中的重要内容。本书旨在加强学生实验基本技能训练，掌握基础和现代分析化学技术