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1、中草药ChineseTraditionalandHerbalDrugs第34卷第9期2003年9月·797·表9HP—Innowax柱上姜黄挥发油GC谱8主峰保留指数数据Table9RetentionindicesofeightmainpeaksinGCchromatogramsofessentialoilinC.longaobtainedwithHP—Innowax柱前压升温速率保留指数/kPa/(℃·min-1)1234567880415851723172917761782219322572272704159017251731177817842197226122778031
2、572171617211769177621852247226370315771719172417721778218822502266平均相对保留值15811721172617741780219122542270RSD/%0.510.230.260.230.210.240.280.28References:[1]RegulationsfortheEstablishmentoftheFingerprintSpectraStandardoftheTCMInjections(Draft)(中药注射剂指纹图谱研究的技术要求(暂行)[S].2000.[2]HongXK,WangZH,Guo
3、JX,etal.Thefingerprintspec-trumanalysisofGCrelativeretentionvaluesforessentialoilof19speciesofBupleurumGenus[J].ActaPharmSin(药学学报),1988,23(11):839-845.[3]KovatsE.GaschromatographiccharacterizationoforganiccompoundsⅠ.Retentionindexesofaliphatichalides,alco-hols,aldehydesandketones[J].HelvChim
4、Acta,1958,41:1915.图2姜黄挥发油HP—Innowax柱GC程序升温测定图谱[4]VanDenDoolH,KratzPD.Ageneralizationoftheretentionindexsystemincludinglineartemperatureprogrammedgas-Fig.2GCchromatogramofessentialoilinC.liquidpartitionchromatography[J].JChromatogr,1963,longaobtainedwithHP—Innowax11:463.不同基质配比对青辛速释贴质量的影响121郑
5、国,罗光亮,彭荣珍(1.暨南大学医学院第六附属医院江门市五邑中医院,广东江门529031;2.深圳市福田区中医院,广东深圳518034)摘要:目的选择以明胶、西黄蓍胶、甘油、聚丙烯酸钠和青黛制备青辛速释贴的最佳基质配比。方法应用正交试验法,分别以粘度、软硬度、清凉感和刺痛感为衡量指标,综合评定不同基质配比下青辛速释贴的质量。结果青辛速释贴的最佳基质配比为明胶∶西黄蓍胶∶甘油∶聚丙烯酸钠∶青黛(8.0∶3.5∶20∶1.3∶3.0)。结论采用青辛速释贴的最佳基质配比可制备质量较佳的青辛速释贴。关键词:青辛速释贴;基质;正交试验中图分类号:R283.6文献标识码:B文章编号:025
6、32670(2003)09079703EffectofdifferentproportionofmatrixonqualityofQingxinSushiTie121ZHENGGuo-shen,LUOGuang-liang,PENGRong-zhen(1.SixthAffiliatedHospital,WuyiHospitalofTCM,MedicalCollegeofJinanUniversity,Jiangmen529031,China;2.FutianHospitalofTCMinShenzhen,Shenzhen518034,China)Abstract:ObjectT
7、oselecttheoptimumproportionofmatrixforthepreparationprocessofQingxinSushiTie(QST)bygelatia,gumtragacanth,glycerol,sodiumacylateandQingdai.MethodsThepro-cesswasstudiedbyorthogonaltestwithviscosity,softandhardmeasurementalgefacientsentation,twingesen
