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1、METHOD8015BNONHALOGENATEDORGANICSUSINGGC/FID1.0SCOPEANDAPPLICATION1.1Method8015isusedtodeterminetheconcentrationofvariousnonhalogenatedvolatileorganiccompoundsandsemivolatileorganiccompoundsbygaschromatography.Thefollowingcompoundscanbedeterminedquantitativelybythismethod:Ap
2、propriateTechniqueCompoundNamePurge-and-DirectSolventaCASNo.TrapInjectionExtractionAcetone67-64-1ppb,dIAcetonitrile75-05-8ppb,dIAcrolein107-02-8ppb,dIAcrylonitrile107-13-1ppb,dIAllylalcohol107-18-6htb,dI1-Butanol(n-Butylalcohol)71-36-3htb,dIt-Butylalcohol75-65-0ppb,dI2-Chlor
3、oacrylonitrile(I.S.)920-37-6NAdNACrotonaldehyde123-73-9ppb,dIDiethylether60-29-7bbI1,4-Dioxane123-91-1ppb,dIEthanol64-17-5Ib,dIEthylacetate141-78-6Ib,dIEthyleneglycol107-21-1IbIEthyleneoxide75-21-8Ib,dIHexafluoro-2-propanol(I.S.)920-66-1NAdNAHexafluoro-2-methyl-2-propanol(I.
4、S.)515-14-6NAdNAIsobutylalcohol78-83-1ppb,dIIsopropylalcohol67-63-0ppb,dIMethanol67-56-1Ib,dIMethylethylketone(MEK)78-93-3ppb,dIMethylisobutylketone(MIBK)108-10-1ppb,dIN-Nitroso-di-n-butylamine924-16-3ppb,dbParaldehyde123-63-7ppb,dI2-Pentanone107-87-9ppb,dI2-Picoline109-06-8
5、ppb,dI1-Propanol71-23-8ppb,dIPropionitrile107-12-0htdICD-ROM8015B-1Revision2December1996AppropriateTechniqueCompoundNamePurge-and-DirectSolventaCASNo.TrapInjectionExtractionPyridine110-86-1Ib,dbo-Toluidine95-53-4Ib,dbaChemicalAbstractServicesRegistryNumber.bAdequateresponseu
6、singthistechniquedAmenabletoconcentrationbyazeotropicdistillation(Method5031)htMethodanalyteonlywhenpurgedat80ECIInappropriatetechniqueforthisanalyteppPoorpurgingefficiency,resultinginhighEQLsNANotavailableI.S.InternalstandardappropriateforMethod50311.2Thismethodmayalsobeapp
7、licabletotheanalysisofpetroleumhydrocarbons,includinggasolinerangeorganics(GROs)anddieselrangeorganics(DROs).GROscorrespondtotherangeofalkanesfromC6toC10andcoveringaboilingpointrangeofapproximately60EC-170EC(Reference6).DROscorrespondtotherangeofalkanesfromC10toC28andcoverin
8、gaboilingpointrangeofapproximately170EC-430EC(Reference6).Theidentification
