EPA 9074 TURBIDIMETRIC SCREENING METHOD FOR TOTAL RECOVERABLE

EPA 9074 TURBIDIMETRIC SCREENING METHOD FOR TOTAL RECOVERABLE

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时间:2019-10-18

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1、METHOD9074TURBIDIMETRICSCREENINGMETHODFORTOTALRECOVERABLEPETROLEUMHYDROCARBONSINSOILSW-846isnotintendedtobeananalyticaltrainingmanual.Therefore,methodproceduresarewrittenbasedontheassumptionthattheywillbeperformedbyanalystswhoareformallytrainedinatleastthebasicprinc

2、iplesofchemicalanalysisandintheuseofthesubjecttechnology.Inaddition,SW-846methods,withtheexceptionofrequiredmethodusefortheanalysisofmethod-definedparameters,areintendedtobeguidancemethodswhichcontaingeneralinformationonhowtoperformananalyticalprocedureortechniquewh

3、ichalaboratorycanuseasabasicstartingpointforgeneratingitsowndetailedStandardOperatingProcedure(SOP),eitherforitsowngeneraluseorforaspecificprojectapplication.Theperformancedataincludedinthismethodareforguidancepurposesonly,andarenotintendedtobeandmustnotbeusedasabso

4、luteQCacceptancecriteriaforpurposesoflaboratoryaccreditation.1.0SCOPEANDAPPLICATION1.1Thismethodmaybeusedtoscreensoilsamplestodeterminethetotalamountofrecoverablepetroleumhydrocarboncontaminationinsoilincludingawiderangeoffuels,oils,andgreases.Theturbidimetricapproa

5、chinthismethodisdesignedtoquicklyscreensoilsamplesusingasystemcalibratedwithablankandasinglecalibrationstandard.1.2ThedefinitionoftotalrecoverablepetroleumhydrocarbonsforthismethodcanbefoundinSec.3.0.1.3Thisscreeningtechniqueisspecificallydesignedtobeusedinthefieldb

6、utmayalsohavesomescreeningapplicationsinthelaboratory.Thesystemanalysisrangeis10-2000ppmformosthydrocarbons.1.4Thismethodisconsideredascreeningtechniquebecauseofthebroadspectrumofhydrocarbonsitdetects.Themethodmaybeespeciallyusefulinquicklydeterminingthatasitedoesno

7、tcontainhydrocarboncontamination.However,itcannotbeusedtodeterminespecifichydrocarboncompoundsorgroupsofcompoundsthatmaybepartofalargerhydrocarbonmixture.Aswithotherscreeningtechniques,itisadvisabletoconfirmacertainpercentageofbothpositiveandnegativetestresults,espe

8、ciallywhennearorabovearegulatoryactionlimitorwhenthepresenceofbackgroundorinterferinghydrocarbonsissuspected.Thelimitationsofthisprocedure

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