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1、METHOD8000BDETERMINATIVECHROMATOGRAPHICSEPARATIONS1.0SCOPEANDAPPLICATION1.1Method8000isnotadeterminativemethodbutinsteadprovidesguidanceonanalyticalchromatographyanddescribescalibrationandqualitycontrolrequirementsthatarecommontoallSW-846chromatographicmethods.ApplyMethod8000inconjunctionw
2、ithallSW-846determinativechromatographicmethods.Themethodsinclude,butarenotlimitedto,thefollowing:MethodChromatographicNumberAnalytesTechnique(seeSec.1.5)Detector7580Whitephosphorus(P4)GC,capillarycolumnNPD8011EDB,DBCPGC,capillarycolumnECD8015NonhalogenatedvolatilesGC,packed&capillaryFIDco
3、lumn8021VolatilesGC,capillarycolumnPID,ELCD8031AcrylonitrileGC,packedcolumnNPD8032AcrylamideGC,packedcolumnECD8033AcetonitrileGC,capillarycolumnNPD8041PhenolsUnderivatizedorFID,ECDderivatized,GC,capillarycolumn8061PhthalatesGC,capillarycolumnECD8070NitrosaminesGC,packedcolumnNPD,ELCD,TED80
4、81OrganochlorinepesticidesGC,capillarycolumnECD,ELCD8082PolychlorinatedbiphenylsGC,capillarycolumnECD,ELCD8091NitroaromaticsandcyclicGC,capillarycolumnECDketones8100PAHsGC,packed&capillaryFIDcolumn8111HaloethersGC,capillarycolumnECD8121ChlorinatedhydrocarbonsGC,capillarycolumnECDCD-ROM8000
5、B-1Revision2December1996MethodChromatographicNumberAnalytesTechnique(seeSec.1.5)Detector8131AnilineandselectedderivativesGC,capillarycolumnNPD8141OrganophosphoruspesticidesGC,capillarycolumnFPD,NPD,ELCD8151AcidherbicidesDerivatize;GC,capillaryECDcolumn8260VolatilesGC,capillarycolumnMS8270S
6、emivolatilesGC,capillarycolumnMS8275SemivolatilesThermalextraction/GCMS8280DioxinsandDibenzofuransGC,capillarycolumnLowresolutionMS8290DioxinsandDibenzofuransGC,capillarycolumnHighresolutionMS8310PAHsHPLC,reversephaseUV,Fluorescence8315CarbonylcompoundsDerivatize;HPLCFluorescence8316Acryla
7、mide,acrylonitrile,HPLC,reversephaseUVacrolein8318N-MethylcarbamatesDerivatize;HPLCFluorescence8321ExtractablenonvolatilesHPLC,reversephaseTS/MS,UV8325ExtractablenonvolatilesHPLC,reversephasePB/MS,UV8330NitroaromaticsandnitraminesHPLC,reversephaseUV8331Tetraze
