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1、METHOD8000CDETERMINATIVECHROMATOGRAPHICSEPARATIONS1.0SCOPEANDAPPLICATION1.1Method8000isnotadeterminativemethodbutinsteadprovidesguidanceonanalyticalchromatographyanddescribescalibrationandqualitycontrolrequirementsthatarecommontoallSW-846chromatographicmethods.However,mo
2、respecificqualitycontrolrequirementsthatareprovidedintheapplicabledeterminativemethodwillsupersedethosenotedinMethod8000.ApplyMethod8000inconjunctionwithallSW-846determinativechromatographicmethods.Themethodsinclude,butarenotlimitedto,thefollowing:MethodChromatographicNu
3、mberAnalytesTechnique(seeSec.1.5)Detector7580Whitephosphorus(P4)GC,capillarycolumnNPD8011EDB,DBCPGC,capillarycolumnECD8015NonhalogenatedvolatilesGC,packed&capillaryFIDcolumn8021VolatilesGC,capillarycolumnPID,ELCD8031AcrylonitrileGC,packedcolumnNPD8032AcrylamideGC,packedc
4、olumnECD8033AcetonitrileGC,capillarycolumnNPD8041PhenolsUnderivatizedorFID,ECDderivatized,GC,capillarycolumn8061PhthalatesGC,capillarycolumnECD8070NitrosaminesGC,packedcolumnNPD,ELCD,TED8081OrganochlorinepesticidesGC,capillarycolumnECD,ELCD8082PolychlorinatedbiphenylsGC,
5、capillarycolumnECD,ELCD8091NitroaromaticsandcyclicGC,capillarycolumnECDketones8100PAHsGC,packed&capillaryFIDcolumn8111HaloethersGC,capillarycolumnECD8000C-1Revision3March2003MethodChromatographicNumberAnalytesTechnique(seeSec.1.5)Detector8121ChlorinatedhydrocarbonsGC,cap
6、illarycolumnECD8131AnilineandselectedGC,capillarycolumnNPDderivatives8141OrganophosphoruspesticidesGC,capillarycolumnFPD,NPD,ELCD8151AcidherbicidesDerivatize;GC,capillaryECDcolumn8260VolatilesGC,capillarycolumnMS8265VolatilesNADSITMS8270SemivolatilesGC,capillarycolumnMS8
7、275SemivolatilesThermalextraction/GCMS8280DioxinsandDibenzofuransGC,capillarycolumnLowresolutionMS8290DioxinsandDibenzofuransGC,capillarycolumnHighresolutionMS8310PAHsHPLC,reversephaseUV,Fluorescence8315CarbonylcompoundsDerivatize;HPLCFluorescence8316Acrylamide,acrylonit
8、rile,HPLC,reversephaseUVacrolein8318N-MethylcarbamatesDerivatize;HPLCFluorescence8321Extractablenonvola
