药物分析实验(药学英语)

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1、SelectedExperimentsofPharmaceuticalAnalysis（药物分析实验/供英语药学使用）EditedbyLiuqianYuZhiguoMay.200341PrefaceThe“SelectedExperimentsofPharmaceuticalAnalysis”isforthestudentsoftheEnglishClassofPharmacy.Thisbookletisthesecondedition.ItwaseditedbyMsLiuQianandMrYuZhiguo.Theexperimentsi

2、ncludedwereselectedfromthefirstedition(1994,byYuZhiguo)andtheChineseedition(2001,byHouXiaohong).LiuQianDepartmentofPharmaceuticalAnalysisMay,200341ContentsExp.1TestsforGenericImpuritiesinGlucose………………………………………01Exp.2TestsforSpecificImpurities…………………………………………………04Exp.3Assa

3、yofCompoundAapirinTabletsbyVolumetricTitrationMethod………07Exp.4AssayofDi-iodohydroxyquinolineTabletsUsingOxygenFlaskCombustion……………………………………………11Exp.5DiphasicTitrationofOrganicBases…………………………………………14Exp.6Non-aqueousAlkalimetricMethodofQuinineSulfate……………………16Exp7Theassayof

4、medicinebyRedoxTitrationMethod………………………18Exp.8Double-wavelengthSpectroscopicAssayofcompoundsulfamethoxazoletablets……………………………………19Exp.9ThevalidationandapplicationofUV-spectrophotometryintheassayofpreparation…………………………………………………22Exp.10ThetestofHPLCsystemsuitabilityandappli

5、cationofHPLCintheassayofpreparation…………………………………………………24Exp.11TheapplicationsofGCintheassayofChinesetraditionalmedicinalmaterials…………………………………27Exp.12Theassayofdruginbiologicalsample（I）——Thefoundationandvalidationofanalyticalmethod…………………29Exp.13Theassayofdruginbiological

6、sample（II）——Theestimationofpharmacokineticparameter………………………3241Exp.1TestsforGenericImpuritiesinGlucosePURPOSEToknowwelltheprincipleoftestsforthegenericimpuritiesTopractisetheproceduresoftestsforimpuritiesPROCEDUREAcidityDissolve2.0gin20mLofwater.Add3dropsofphenolphthalei

7、nTSand0.20mLofsodiumhydroxidesolution(0.02mol/L).Thesolutionproducesadistinctpinkcolor.ClarityandcolorofsolutionDissolve5ginsufficienthotwater,cool,anddiluteto10mLwithwater.Thesolutionisclearandcolorless.Ifthesolutionisopalescent,theopalescenceofthesolutionisnotmoreintens

8、ethanthatofNo1TurbidityStandardSolution;Ifthesolutioniscolored,thecolorofthesolutionisnotmoreint