甲乙酮催化剂的制备及工艺研究

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1、分类号：——UDC：——Y936007密级：——编号：——工程硕士学位论文甲乙酮催化剂的制备及工艺研究硕士研究生指导教师企业导师学位级别学科、专业所在单位论文提交日期论文答辩日期学位授予单位：刘斌：李占双副教授：张学路高级工程师：工程硕士：化学工程：化工学院：2006年1月：2006年3月：哈尔滨工程大学j哈尔滨～Ij程火学I‘程硕士论文AbstractMethyl—ethylkctone(MEKshortfor)isanimportanto唱aJlicsolVentwithexcellentproperty

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3、cineindustry．Besides，iccanbealsousedforprcparingVariousdope，adhesive，printingi11ketc．Nowitsusabilitywasextendedtot印eproducinginelectmnicindus仃yandpfimingcircuitrymanufkturing．Itisalsoa11import跗Cmaterialfbro略anicsynthesis，wllichcaIlbeusedtoprepareMEKperoxide

4、，MEKhydroximinoetc．andaninte珊ediateforprcp撕ngspice，aIltioxidanta11dsomecatalyst．Basedont11eWidelyuseofMEK，wechooseMEKastheultimateproductantin01】rresearchaIlduseanadvancedindllstrymethod——n．butenyldirectlyhydrationtoprepareSBA粕dSBAdehydIDgenationtopreparcME

5、K．Usingstyrcne，divinylb蚴easrawmat硎alsandusingp01ymerizing，abs仃acting，bromizin舀smph嘶zing，actiVegr。1巾stabilizationaStecllIliqueprocess，theDNWresincalalystissynmesiZed，andthiscatalystisusedincatalyzingtheprocessofprep“hgSBA．nlephysicalstnlctureaIldmoIecularco蠲

6、gu豫耍on，anditsrelatiVity谢也heatresist锄ceisstudiedby2400n出()南cL13CNMR，static，dyn锄icheatstabilityteSt，andsoon．Thepreparationartisimprovedandt11eactivityaswellastheheatstabilityofDNWresincatalystwepr印aredareequalorsuperio“othecouIltc芏panintheworld．ThecatalyStisu

7、sedintheprocessofpreparingSBAt11rou曲n出utylenehydration，andtheanconditionisalsoinVestigated．DuringthcdehydrogenpreparationoftheMEKwithsBA，theactiVityofthe哈尔滨]一程大学T程硕士论文f0衄ercatalyzerSisnotsogood，thesarneasthoseaIlticongregateca而on，Theintensityandthewearabili

8、tyofthemechaIlismislowwhichresultinitsonlycontainingCuO—zn0，withoutfeltion．Anditsintens时islowaftermoulding．Itstcxnlreiscompactandt11ecosurfaceislowInordertoimplementandimproveitsindustrialization，there