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1、AllenHunter’sYSUX-RayStructureSolutionLabManual:ABeginner’sIntroductionI-1ALLENHUNTER’SYOUNGSTOWNSTATEUNIVERSITYX-RAYSTRUCTUREANALYSISLABMANUAL:1ABEGINNER’SINTRODUCTIONOPTIMIZEDFORUSEWITHSHELXTLANDDOSDr.AllenD.HunterProfessorofChemistryDirectoroftheYSUS
2、tructureCenterDepartmentofChemistryYoungstownStateUniversity1UniversityPlaza,YoungstownOhio44555-3663adhunter@cc.ysu.eduhttp://www.as.ysu.edu/~adhunter/index.htmlWinter1999DraftRelease:VersionW99D1DetailedCommentsOnThisDraftManualAreRequestedFromAllUser
3、sthth©Dr.AllenD.Hunter,March241997andOctober27,1998.1ThislabmanualisbasedontheauthorsexperienceteachingcrystallographytoundergraduatesandMSstudentsatYoungstownStateUniversity,hisexperiencewiththesoftware,theSHELXTLmanual(Version5.1)fromBrukerAXS(Siemens
4、),GeorgeSheldrick’sSHELXmanuals,aswellastheotherreferenceslistedintheappendix.Winter1999D1Edition,ForInstructionalUse,UseOnlyWithTheAuthor’sPermissionAllenHunter’sYSUX-RayStructureSolutionLabManual:ABeginner’sIntroductionI-2INFORMATIONABOUTTHEUSERLICENS
5、EThislaboratorymanualwaswrittenbyDr.AllenD.HunteroftheYoungstownStateUniversityChemistryDepartmentfrom1996tothepresent.Theauthorretainssolecopyrighton2thismanualinbothitsprintedandelectronicforms.Whetheryouobtainedthismanualdirectlyfromhim(i.e.,asaregis
6、tereduser),throughtheagencyofaregistereduser,orthroughoneormoreintermediaries,thefollowinglicenseinformationappliestoyou.Byusingthismanualforyourteaching,research,orotherpurposesyouareacceptingthetermsofthislicenseagreement.st3Thetermofthisagreementexpi
7、resonDecember31,2000.Thislaboratorymanualisprovidedfreeofchargeforuseinbothteachingandresearchtoeducationalandnon-profitinstitutions.Corporateusersareaskedtocontacttheauthoraboutanyfees,whichwilldependuponthenatureoftheintendeduse.Thesourcefilesforthema
8、nualmaynotbeedited/rewritten,however,handwrittenannotationsbeforeprintingareallowedandareevenencouragedtomakethismanualofmoreusetoyourstudents.Thesoleexceptiontothisrestrictionisthatlicensedusersmayfreelyelecttoduplicateanddistri
