氯吡格雷(OJ)

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1、DAICELCHIRALTECHNOLOGIES(CHINA)CO.,LTD.Column:CHIRALCELOJ-H（NE004）Columnsize:0.46cmI.D.×25cmLInjection:10μlMobilephase:n-Hexane/IPA/DEA=95/5/0.1(v/v/v)Flowrate:1.0ml/minWavelength:UV240nmTemperature:25℃Samplesolution1.0mg/mlinHexaneIPAHPLCequipment:ShimadzuLC20withUVdetectorSPD

2、-20ASamplestructureA100811B混合PeakNo.TimeAreaArea%PlatenumberTailingResolution16.511484976936.70281020.3402.218--214.230151315311.45153249.7611.1438.512317.031315413923.87043635.4701.1882.632421.345157701711.93483566.9801.1633.371536.115211

3、953016.04053448.5411.1087.5955DAICELCHIRALTECHNOLOGIES(CHINA)CO.,LTD.Column:CHIRALCELOJ-H（NE004）Columnsize:0.46cmI.D.×25cmLInjection:4μlMobilephase:n-Hexane/IPA/DEA=95/5/0.1(v/v/v)Flowrate:1.0ml/minWavelength:UV240nmTemperature:25℃Samplesolution2.5mg/mlinHexaneIPAHPLCequipment:

4、ShimadzuLC20withUVdetectorSPD-20ASamplestructureA100811B主药PeakNo.TimeAreaArea%PlatenumberTailingResolution117.111355280.37653845.2551.756--221.377295990.31375366.9121.6123.757335.809937082399.30983197.8981.2267.8015DAICELCHIRALTECHNOLOGIES

5、(CHINA)CO.,LTD.PColumn:CHIRALCELOJ-H（NE004）Columnsize:0.46cmI.D.×25cmLInjection:10μlMobilephase:n-Hexane/IPA/DEA=95/5/0.1(v/v/v)Flowrate:1.0ml/minWavelength:UV240nmTemperature:25℃Samplesolution0.8mg/mlinHexaneIPAHPLCequipment:ShimadzuLC20withUVdetectorSPD-20ASamplestructureA100

6、811B杂质APeakNo.TimeAreaArea%PlatenumberTailingResolution16.5327791207100.00001022.9872.216--5DAICELCHIRALTECHNOLOGIES(CHINA)CO.,LTD.Column:CHIRALCELOJ-H（NE004）Columnsize:0.46cmI.D.×25cmLInjection:10μlMobilephase:n-Hexane/IPA/DEA=95/5/0.1(v/

7、v/v)Flowrate:1.0ml/minWavelength:UV240nmTemperature:25℃Samplesolution0.9mg/mlinHexaneIPAHPLCequipment:ShimadzuLC20withUVdetectorSPD-20ASamplestructureA100811B杂质BPeakNo.TimeAreaArea%PlatenumberTailingResolution114.152517058450.26983082.9451

8、.188--221.226511507349.73023490.1721.2265.759Testingda