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1、METHOD8330BNITROAROMATICS,NITRAMINES,ANDNITRATEESTERSBYHIGHPERFORMANCELIQUIDCHROMATOGRAPHY(HPLC)SW-846isnotintendedtobeananalyticaltrainingmanual.Therefore,methodproceduresarewrittenbasedontheassumptionthattheywillbeperformedbyanalystswhoareformallytrainedinatleastthebasicprinciple
2、sofchemicalanalysisandintheuseofthesubjecttechnology.Inaddition,SW-846methods,withtheexceptionofrequiredmethodusefortheanalysisofmethod-definedparameters,areintendedtobeguidancemethodswhichcontaingeneralinformationonhowtoperformananalyticalprocedureortechniquewhichalaboratorycanuse
3、asabasicstartingpointforgeneratingitsowndetailedStandardOperatingProcedure(SOP),eitherforitsowngeneraluseorforaspecificprojectapplication.Theperformancedataincludedinthismethodareforguidancepurposesonly,andarenotintendedtobeandmustnotbeusedasabsoluteQCacceptancecriteriaforpurposeso
4、flaboratoryaccreditation.1.0SCOPEANDAPPLICATION1.1Thismethodisintendedforthetraceanalysisofexplosivesandpropellantresiduesbyhighperformanceliquidchromatography(HPLC)usingadualwavelengthUVdetector.ThefollowingRCRAcompoundsinawater,soil,orsedimentmatrixhavebeendeterminedbythismethod:
5、aAnalyteAbbreviationCASNumberOctahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocineHMX2691-41-0Hexahydro-1,3,5-trinitro-1,3,5-triazineRDX121-82-41,3,5-Trinitrobenzene1,3,5-TNB99-35-41,3-Dinitrobenzene1,3-DNB99-65-0Methyl-2,4,6-trinitrophenylnitramineTetryl479-45-8NitrobenzeneNB98-95-32,4
6、,6-Trinitrotoluene2,4,6-TNT118-96-74-Amino-2,6-dinitrotoluene4-Am-DNT19406-51-02-Amino-4,6-dinitrotoluene2-Am-DNT35572-78-22,4-Dinitrotoluene2,4-DNT121-14-22,6-Dinitrotoluene2,6-DNT606-20-22-Nitrotoluene2-NT88-72-23-Nitrotoluene3-NT99-08-14-Nitrotoluene4-NT99-99-0NitroglycerinNG55-
7、63-0PentaerythritoltetranitratePETN78-11-53,5-Dinitroaniline3,5-DNA618-87-18330B-1Revision2October2006aChemicalAbstractServiceRegistryNumber1.2Thismethodprovidesadirectinjectionprocedureforhighlevelwatersamples,anextractionprocedureforsoilsandsedimentsaswellasalowlevelmethodforthee
8、xtractionofwatersamples.Th
