GBT16631-1996 柱液相色谱分析法通则.pdf

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1、ICS71.040.40c04E中华人民共和国国家标准GB/T16631一1996柱液相色谱分析法通则Generalrulesforanalyticalmethodsofliquidcolumnchromatography1996一12一02发布1997一05一01实施国家技术监督局发布GB/T16631一1996目一次前言、苦工范围······，，·········，·‘·······，··‘····，··“···，，，，···，·········，，，，·”··中”，····，···”····““，·”二1q‘引用标准·...................

2、.....................................................................................·一1︹口方法概要·.............................................................................................................1乙仪器·...........................................................................

3、.........................................1巴口流动相·................................................................................................................3心U柱填充剂·································，，，·········，·，·········，”··········，，································，，，·⋯6月2试验前的准备

4、工作·..................................................·一，····⋯⋯，···········.·..·..·..·.⋯⋯9卜匕10操作······，··⋯0l0矽色谱柱的评价10色谱图的整理··················································“······················“···············⋯⋯1111定性分析················”···············，··········，···········”······

5、···········，，·”·················⋯⋯n12定量分析·.....................................................................................................·一1113分子量的测定··············，····“··································，.····································“⋯⋯11附录A(提示的附录)用于液相色谱法中溶剂的性质······，··

6、···，，，····‘···，，············”·······，·⋯13附录B(提示的附录)二元溶剂体系的组成与其强度的关系·······”·······················”··”····一15附录C(提示的附录)溶剂的选择性三角坐标·························································⋯⋯16附录D<提示的附录)离子交换色谱法中常用的缓冲剂·.....................................................17附录E(提示的附录)柱填充剂

7、··································”，.，···，···················.·..·..·..·..·.⋯⋯18附录F(提示的附录)化学键合相柱填充剂······，·····“············，.·”·········，····”··············⋯⋯19附录G(提示的附录)环境要求·..................................................................................21附录H(提示的附录)安全要求··········

8、···。”·······