复方扶芳藤胶囊质量控制方法的研究

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1、目录中文摘要···················································1英文摘要···················································3引言························································6正文························································7第一部分复方扶芳藤胶囊的制备············

2、···············71.实验材料·················································71.1实验样品·················································71.1.1药材与药品··············································71.1.2主要仪器·················································72.实验方法·······

3、············································7第二部分复方扶芳藤胶囊指纹图谱研究··················9第一节复方扶芳藤胶囊成品和中间体的指纹图谱研究···91.实验材料·················································91.1实验样品·················································91.1.1药品······························

4、······················91.1.2药材····················································91.1.3试剂····················································91.1.4主要仪器················································91.1.5分析软件···············································1

5、02.实验方法················································102.1供试品溶液的制备····································102.1.1提取方法的考察····································102.1.2洗涤方法的考察····································112.1.3溶剂用量的考察····································132.

6、1.4提取时间的考察····································132.2对照品溶液的制备····································142.3色谱条件的选择······································152.3.1色谱柱选择·········································152.3.2检测器及其参数的选择·····························172.3.3柱温选择···

7、········································192.3.4进样量选择·········································202.3.5流动相的选择·······································202.3.6色谱条件与系统适用性试验························232.4复方扶芳藤胶囊指纹图谱方法学考察·················232.4.1仪器精密度试验··················

8、···················232.4.2重复性试验·········································252.4.3样品稳定性试验····································273.实验结果················································293.1样品的测定······