微波场中3-氯-2-羟基丙磺酸钠的合成与其表征

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1、2.4.1微波辐射温度对产物收率的影响....................................................172.4.2微波辐射时间对产物收率的影响....................................................182.4.3催化剂用量对产物收率的影响........................................................192.4.4反应物摩尔比对产物收率的影响.............

2、.......................................202.4.5溶剂水用量对产物收率的影响........................................................212.5不同磺化剂对产物收率的影响..................................................................222.6滴加顺序对反应收率的影响......................................

3、................................232.6.1微波辐射温度对反应收率的影响....................................................232.6.2微波辐射时间对反应收率的影响....................................................232.6.3反应物摩尔比对反应收率的影响....................................................242

4、.6.4催化剂用量对反应收率的影响........................................................242.7催化剂种类对反应收率的影响..................................................................242.7.1微波辐射温度对反应收率的影响....................................................252.7.2微波辐射时间对反应收率的影响...

5、.................................................252.7.3摩尔比对反应收率的影响................................................................252.7.4催化剂用量对反应收率的影响........................................................262.8正交试验设计与优化.................................

6、.................................................262.8.1设计正交实验表................................................................................262.8.2分析结果并讨论................................................................................272.9本章小结........

7、..............................................................................................28第3章常规条件下合成3-氯-2羟基丙磺酸钠的研究.........................................293.1实验方法....................................................................................

8、..................293.1.1主要试剂和仪器................................................................................293.1.2实验过程............................................................................................293.1.3