华中碎米荠化学成分与其质量标准的初步-.研究

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1、conditionsincludingextractionmethod，extractionsolventanddevelopingagent，fina1lytheprogramiSsetwithsi1icagelGplate，chloroform—ethylacetate—methanol—water(15：40：22：10)placed10℃belowtoclarifythelowersolutionasdevelopingagent，spraying10％sulfuricacidinethanol，heatedtoaclearspotcolorat105℃，respecti

2、vely，setdaylightandUV1ight(365nm)toview．Theproductchromatography，andthecontroldruginchromatOgraphiccorrespondingplace，respectivelyshowthesamecolorofthespotorfluorescentspots．TheidentificationmethodisSimple，convenient，quick，Strongreproducibi1ityandtheresultsarerellable．Thecontentoftota1saponin

3、sinCardamineUrbaniana0．E．SchlziSdetectedbytheUV—ViSiblespectrophotometry．ThemethodtopreparesolutionofproductisdeterminedaftersearchofitSextractionmethod，solventmultiPles，thenumberofextraction．andextractiontime．With01eanoliCacidasreferencesubstance，thecontentoftotalsaponinsisdetectedbytheUV-vi

4、Siblespectrophotometryat547nmwavelength，meanwhilecorrespondingmethodologyinvestigationiScarrledout．Bymeasuringthefivebatchesofsamples，tentativelysetproductoftotaIsaponinsshouldnotbe1essthan1．81％．AccordingtothepharmacopoeiaofthePeople7SRepublicof2010versionofthemeasurementmethodoftheappendix，r

5、espectivelyexaminetheV01ati1eoi1content，moisture，tota1ashandacidinsolubleashofCardamine纷baniana0．E．Schlz．Thus，themethodisaccurate，reliable，reproducible，whichcanpre1iminaryestablishaqualityevaluationsystemofCardamineUrbaniana0．E．Schlz．ChemicalconstituentsandqualityStandardofCardamineVUrbaniana

6、0．E．Schlzaresystematica1lyinvestigated．Itisidentifled75volatilecompounds．OnthebasiSofaboveexperimentalresultS，qua1ityspecificationdraftandadditionalremarksdetai1edindraftwasworkedout．ItprovidestheSClentificbasesforthequalityof饧rdamine0．E．Schlz，anditestablishesacertainfoundationtodeepenitsStud

7、y．A11theseachievementsareofgreatSignificanceforrationa1developmentandutilizationof饧rdamineUrbaMann0．E．Sch1z．KeywordsCardamine0．E．SchIZ：ChemicaIconstituent：Qualitystandards：VoIatiIeconstituents：TotaIsaponinsVIO．E．Schlz)l均干燥根茎，具有特异性的香气，有止咳、化痰、活