B2O3金属氧化物固体酸催化单糖转化5羟甲基糠醛(HMF)

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1、-贵州大学2015届硕士研究生学位论文5.1Al2O3-B2O3催化剂制备方法......................................................................................................................495.2Al2O3-B2O3催化剂的表征.................................................................................

2、.........................................505.2.1热重分析.............................................................................................................................................505.2.2傅里叶红外光谱（FTIR）分析............................................

3、............................................................505.2.3X-射线粉末衍射（XRD）分析.........................................................................................................515.2.4扫描电子显微镜(SEM)、透射电子显微镜（TEM）分析......................................

4、..................535.2.5AlnB10-n的NH3-TPD及吡啶红外分析.............................................................................................545.2.6N2-吸附脱附分析及ICP-AES分析............................................................................................

5、.......565.3Al2O3-B2O3催化葡萄糖转化HMF............................................................................................................575.3.1Al2O3-B2O3与同源催化剂的对比.............................................................................................

6、.........575.3.2不同摩尔比催化剂的筛选.................................................................................................................585.3.3温度、时间对Al-B催化葡萄糖转化HMF的影响........................................................................605.3.4催化剂Al2O3-B

7、2O3(nAl:nB=5:5)的量对反应的影响...................................................................635.3.5DMSO用量对葡萄糖转化HMF的影响...........................................................................................645.3.6不同溶剂对反应的影响....................................

8、.................................................................................655.3.7Al5B5催化葡萄糖转化HMF反应体系中可能副产物的确定..........................................................665.3.8葡萄糖异构化