xray crystallography facility overviewklb型x射线晶体学设施概述课件

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1、Welcome!X-RayFacility,410-413KashaLaboratoryInstituteofMolecularBiophysicsFloridaStateUniversityTallahassee,FL32306-4380www.sb.fsu.edu/~xrayãThayumanasamySomasundaram,2003-2004X-RayFacilityOrientationHistoryoftheFacilityFacilityResourcesRequirementsDataCollectionDataProc

2、essing&ManualsArchiving&SummaryContact&InformationãThayumanasamySomasundaram,2003-20049/17/20212HistoryoftheFacility-1Corefacilityplannedin1990-92FacilityDirectorhiredFeb1993ConstructionJune–Sep1993Twogenerators&ImagePlate(IP)detectorinJanuary1994Elliottgeneratorin1995Im

3、portantDatesãThayumanasamySomasundaram,2003-20049/17/20213HistoryoftheFacility-2Cryocapabilitiesin1996Crystalchamberin1999ConfocalmirrorinSpring2000CCDw/confocalmirrorinFall2000CryoCooler700w/auto-refillinFall2000AdditionalLinuxmachinesin2000Completerenovationduring2002-

4、03ImportantDatesãThayumanasamySomasundaram,2003-20049/17/20214FacilityResources&AccessoriesThreeCopperrotatinganodegeneratorsTwoautomatedareadetectorsTwoconfocal&onetotalreflectionmirrorsTwocryocoolersOneautomatedliquidNitrogenrefillerLinuxandWindowsNTcomputersFulltimeFa

5、culty/Staff(State-line)ãThayumanasamySomasundaram,2003-20049/17/20215Resources-1GeneratorsTwoRigakuH2R5.4kWgeneratorsOneElliottGX-303.0kWgeneratorAreadetector-1(IP)R-AxisIIc(1994)w/confocalbluemirror65-450mmsample-detectordistance0-25degreenon-zero2-thetacapabilityOxford

6、Cryostream600coldheadãThayumanasamySomasundaram,2003-20049/17/20216Resources-2Areadetector-2(CCD)Mar165CCDw/confocalpurplemirror35-380mmsample-CCDdistanceLimitednon-zero2-thetacapabilityOxfordCryostream700coldheadLong&shortSupper(total-reflection)mirrorsStand-aloneIPBioU

7、nitIAnalyticalLabãThayumanasamySomasundaram,2003-20049/17/20217Accessories-1Leicastereomicroscopew/MoticamdigitalcameraNikonOptiphotmicroscopew/analogcameraStereozoommicroscopesDVD-R&+RwritersDDS-3&-4tapedrivesFireWire(Maxtor:60&80GB)drivesWindowsNTandfiveLinuxcomputersã

8、ThayumanasamySomasundaram,2003-20049/17/20218Accessories-2Coldroomfor4°Ccrystallizationset-upRoomforamb