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《高效液相使用方法（high performance liquid phase method）》由会员上传分享，免费在线阅读，更多相关内容在教育资源-天天文库。
1、高效液相使用方法（Highperformanceliquidphasemethod）Usagemethod：(I)switchon:1.Turnonthecomputer,entertheWindowsNT(orWindows2000)screen,andruntheBootpServerprogram.2,open1100LCeachmodulepowersupply.3,aftereachmoduleself-testcompleted,double-clicktheInstrument1Onlineicon,thechemicalworkstationautomaticallycommu
2、nicatewith1100LC,entertheworkstationscreenasfollows.4,fromthe"View"menu,select"MethodandRuncontrol"screen,click"View"menuinthe"ShowTopToolbar","ShowstatusToolbar","Systemdiagram","Samplingdiagram,"thecommandbeforethe"V"logo,toinvokethedesiredinterface.5.Putthemobilephaseintothesolventbottle.6.Turnon
3、thePurgevalve.7,clickthePumpicon,appeartheparametersettingsmenu,clicktheSetuppumpoption,enterthepumpeditscreen.8,setFlow:5ml/min,clickOK.9,clickonthePumpicon,theparametersettingsmenu,clickthePumpcontroloption,selecttheOn,clickOK,thesystembegantoPurge,untilthepipeline(bysolventbottletothepumpentrance
4、)nobubbles,switchingchannelscontinuetoPurge,withnobubbleuntilallchannelssofar.10,clickthePumpicon,appeartheparametersettingmenu,clickthePumpControloption,selectOff,clickOk,turnoffthepump,andturnoffPurgevalve.11,clickthePumpicon,appeartheparametersettingsmenu,clicktheSetuppumpoption,enterthePumpedits
5、creen,setFlow:1.0ml/min.12.Clickthebottleiconbelowthepump,asshown(taketwoyuanpumpasanexample),theactualvolumeoftheinputsolventandthevolumeofthebottle.Youcanalsoenterthevolumeofthestoppump.ClickOk.(two)datacollectionmethodediting:1.Starteditingthefullmethod:FromtheMethodmenu,select"Editentiremethod",
6、asshownabove,selectthethreeitemexcept"Dataanalysis",clickOk,andmovetothenextscreen.2,methodinformation:AddinginformationaboutmethodsinMethodComments(e.g.,methods,uses,etc.).ClickOktoenterthenextscreen.3,pumpparametersetting:(taketwoyuanpumpasanexample)Entertrafficat"Flow",suchas1ml/min,enter"70"("A=
7、100-B")at"SolventB"and"Insert"line"Timetable",editthegradient.AtPressureLimitsMax,enterthemaximumresistanceofthecolumntoprotectthecolumn.ClickOktoenterthenextscreen.4.Automaticsamplerparametersetting:
