nvf-st共聚物的无皂乳液聚合及水解反应

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1、NVF-ST共聚物的无皂乳液聚合及水解反应19NVF-ST???????????????????T???s???????M?????7?U?C???T?????T?N?r???D???)?????????7????????350007?3?????[?????K???9?1?W???????X?2???;?7??????N-???????p????(NVF)?????????TST?3?????????????T?]?N?????2???;?c?????????c?????????????D?????????7???

2、?????NVF-ST?????????s??????k9???????)?7??NVF?)ST???c?????X5?[5k1?????c???????X30%k1?2???;?c???X1%???7?????????D???X90%???5??NVF-ST???????]?c-NHCHO?)NaOH?????:???X1:2???????0?7NVF-ST???????s????????100%k9???D?j?o???)NVF?)DADMAC?????6???????7???s???????b???c?c??k

3、9???K???[???o?????T?]N?????????p?????]???D???]?s??????N-???????p????(NVF)???X?????????b?????????H??,?W??????????????????????????????[1]k9???W?L?S?e?c?????T?????U?????7NVF???w????PNVF?o?????5???p???????c???D???????c?0?a?s???H?c??[2]?7???H?X?L?S????????(PVAm)???=

4、???b????k9PVAm???X?????????????T?H???[?3?????r?????D???????7?????????c???????T?Hk1?????j????[3]k9???DNVF???????,??????k1??????k1???????????j?r?[???????????7?:?????=?r????[4]?7?o??NVF???3???x?,?????????????????????????T?r?7?W?????r???M?9?????;?????T???????7?????

5、??????????????3?????r[5],???????????c???s?V?-k1?????;k1?I??k1?????????)?v?y?j?????7???k????????????k9????NVF?????o?????T[6]???????G???c???K???2???;?7?????K???9?1?U?????K???9?1???O???????7?z???F?3???7???c?(????k9?G???????K???9?1?W???????TAIBA??2HCl?3?X?2???;?7??

6、?c???????????T[7-10]?7????NVF-ST???????TPNVF-ST?3?[?????T???r?ck9?N?????????h???7?????c?????????2???;?c???j???I?????T???0?b???D?????????7????????PNVF-ST???s??????k9?XNVF?????c????????????k91?????-1.1?=?????;??????NVF?7????Sigma-Aldrich,Inc.?????]???????7???[???

7、7???????????????]AIBA??2HCl?7????Sigma-AldrichChemieGmbH?????]???????????????TPVSK?3?7???GWakopurechemicalsIndustries?7Ltd?????]?p??????k1???s?????w?X?-????k9???????????7?5???=???a?X???]DZF??6021???6?????????7?5?????????????S?3???????]Avatar360FTIR?7????Nicolet

8、????k91.2PNVF-ST???T?H?C???3?h????k1?F?????????????????????????b?7?3????????????NVF??ST?7?????????s?7?c?F???0?w?h?k?????h???7?[?K?:30?-???)?????2???;?7???1?????h???u??k91.3?