A twist on packing analytical columns for reversed phase liquid chromatography.pdf

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1、THEFLORIDASTATEUNIVERSITYCOLLEGEOFARTSANDSCIENCESATWISTONPACKINGANALYTICALCOLUMNSFORREVERSEDPHASELIQUIDCHROMATOGRAPHYByJ.PAULMCCALLADissertationsubmittedtotheDepartmentofChemistryandBiochemistryinpartialfulfillmentoftherequirementsforthedegreeofDoctorofPhilosophyDegreeAwarded:FallS

2、emester,2004ThemembersoftheCommitteeapprovetheDissertationofJ.PaulMcCalldefendedonOctober7,2004._________________________JohnG.DorseyProfessorDirectingDissertation_________________________JodeeL.DorseyOutsideCommitteeMember_________________________WilliamT.CooperCommitteeMember____

3、_____________________AlbertE.StiegmanCommitteeMemberTheOfficeofGraduateStudieshasverifiedandapprovedtheabovenamedcommitteemembers.iiiTABLEOFCONTENTSListofTables................................................................................................viListofFigures...........

4、.....................................................................................viiAbstract......................................................................................................ix1.IntroductionandBackground.......................................................

5、..................11.1Introduction...........................................................................................11.2DifferentMethodsforPackingRPLCColumns...................................21.2.1AxialCompression...........................................................

6、............31.2.2RadialCompression.....................................................................41.2.3SlurryPacking..............................................................................51.3DescriptorsofColumnPerformance...............................................

7、.....61.4HeterogeneityFoundWithinthePackedBedsofCurrentRPLCColumns...........................................................................................81.5ResearchGoals......................................................................................131.5.1CentripetalForc

8、easaToolforPackingRPLCColu