中药白附子和娑罗子的化学成分研究及白附子脑苷a的全合成-生药学专业毕业论文

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1、ListofabbreviationsCI．MSChemicalIonizationMassSpectrumCOSYCorrelationSpectroscopyDBU1，8-Diazabicyclo[5，4，O]undec一7一eneDCCDicyclohexyIcarbodiimideD．GalD—galactoseD—GIuD—glucoseD1BAL—HDiisobut，rlaluminiumhydrideDMAP4一N．N—dimethylaminopyridineDMFN，N—dimethylfo

2、rmamideEI—MSElectronImpactMassSpectrumESI．MSElectronSprayIonizationMassSpectrumFABMSFastAtomBombardmentSourceHMBCHeteronuclearMultipleBondConnectivityby2DMultiple—quantumCoherenceHMPAHexamethylphosphoramideHMQC1H—DetectedHeteronuclearMultiple—QuantumCoheren

3、ceviaDirectCouplingHOBt1一HydroxybenzotriazoleHPLCHighPerformanceLiquidChromatographyHR—MSHighResolutionMassSpectrumIRInfraredNMRNuclearMagneticResonancePDCPyridiniumDichromatePrepHPLCPreparativeHighPerformanceLiquidChro——matographyP。T§OHP—Toluenesulfonicaci

4、dRtRetentiontimeSI．MSSecondaryIonMassSpectrumTLCThinLayerChromatographyTrClTriphenylmethylchorideTOF．MSTimeofFlyingMassSpectrumListofTablesTable1．1SomespeciesofTyphoniumgenususedas17drugsandherbaldrugsinChinaTable1-2Somecerebrosidesfoundinnaturalresources24

5、Table1-3Somecatalystusedintheacylatingreaction34Table1—4Someglycosyl．groupsusedintheglycosidation35Table2-1TheConstituentsisolatedfromTyphonium43giganteumEn91．Table2-2NMRdataforTyphonosideA(1)(500MHzfor521Hand125MHzfor13CNMRinCsDsN)Table2-3NMRdataforTyphono

6、sideB(2)(500MHzfor541Hand125MHzfor”CNMRinC5D5N)Table2．4NMRdataforTyphonosideC(9)(500MHzfor561Hand125MHzfor13CNMRinC5D5N)Table2-5NMRdataforTyphonosideD(10)(500MHzfor611Hand125MHzfor13CNMRinC5D5N)Table2-6Theresultsofsomechemicalconstituents63experimentsTable2

7、-7TheconstituentsseparatedbyPrep—HPLC693Table2—8Thetypesofsomecerebrosidestructures8lTable2．9Theexperimentofanti—bloodcoagulation，90viscosityofbloodandplasmaviscosity(Tweenasthereference)Table2．10TheexperimentforT901l—lAofanti—blood90coagulmion，viscosityofb

8、loodandplasmaviscosityTable2-11TheexperimentforX9004··3ofanti·-blood91coagulation，viscosityofbloodandplasmaviscosityTable2-12TheexperimentsforT9004—3，T901卜IAon91bloodviscosityTable2-13TheexperimentforT