规整填料在高压下传质效率的实验研究.pdf

规整填料在高压下传质效率的实验研究.pdf

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1、第20卷第4期吉林化工学院学报VoI.20No.42003年12月JOURNALOFJILININSTITUTEOFCHEMICALTECHNOLOGYDec.2003!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!文章编号:1007-285(32003)04-0001-04THEEXPERIMENTALSTUDYONTHEEFFICIENCYOFSTRUCTUREDPACKINGATHIGHPRESSURE张鹏1,王琨1,高维平1,余

2、国琮2(1.JiIinInstituteofChemicaITechnoIogy,JiIinCity132022,China;2.ChemicaIEngineeringResearchCenter,TianinUniversity,Tianin300072,China)Abstract:MasstransferefficiencyofMeIIapak250YcorrugatedstructuredpackingindistiIIationcoIumnatoperatingpressuresfrom0.3to1

3、.9MpawasstudiedexperimentaIIyandanaIyzedbyusingHTU-NTUmethod.ThedistiIIationcoIumnis0.15mindiameterwithn-butane/n-pentaneasseparatingsystemattotaIrefIux.TheHTUOGisevaIuatedfromthedataofn-butaneconcentrationprofiIeinIiguidphase.OurresuItshowsthattheHTUOGisin

4、creasedfrom0.365to0.551mwithpressureincreasingfrom1.0to1.9Mpa.ItindicatesthereductionofmasstransferefficiencyofthestructuredpackingathighpressureismainIyduetotheeffectofvaporbackmixingandthesubseguentIiguidmaIdistribution.Kwords:masstransfer;structuredpacki

5、ng;backmixing;heightofatransferunit中图分类号:TO050.4+5文献标识码:ACorrugatedmetaIsheetstructuredpackingposeofthispaperistoguantifytheeffectofback-havebeenwideIyusedinthechemicaIandpetro-mixingonmasstransferefficiencyindistiIIationchemicaIindustriessincetheseventiesf

6、ortheircoIumnwithcorrugatedstructuredpackingunderhighthroughput,Iowpressuredrop,IowerIiguidhighpressure.hoIdup,goodseparationefficiencyand,particuIar-Iy,smaIIerscaIe-upeffectincomparisonwithran-1ExperimentaIWorkdompacking.However,fortheappIicationofthestruc

7、turedpackingtohighpressuredistiIIation,theAschematicdrawingofthehigh-pressuredis-observedmasstransferefficiencywasoftenmuchtiIIationcoIumnisshowninFig.1.Theinsidedi-Iowerthanexpected.RecentIy,FRIpubIishedtestameteris150mmandthepackedbedheightisdataforMeIIap

8、ak250Yfortheisobutane/n-butane2000mm.TheoperatingtemperatureismeasureddistiIIationatpressuresfrom0.7~2.7Mpa(Fitzatthetop,middIeandbottomofthecoIumnbythe[1]).At0.7Mpa,theHETpwasfoundtobeetaIresistanceth

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