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1、PesticideAnalyticalManualVol.ISECTION100Chapter1RegulatoryOperationsChapter2GeneralAnalyticalOperationsandInformationChapter3Chapter4MulticlassSelectiveMRMsMRMsChapter5GLCChapter6HPLCTableofContentspagedate301:MulticlassMRMs:ConceptandApplication301A:RecommendedApplicationofMulticlass
2、MRMs301-11/94301B:CapabilitiesandLimitationsofMRMs301-41/94InfluenceofSolventsonMethodology301-41/94Extraction301-41/94Cleanup301-61/94DeterminativeSteps301-71/94References301-71/94302:MethodIforNonfattyFoodsBasicReferences302-11/94GeneralPrinciples302-11/94Applicability302-11/94Metho
3、dModules302-11/94Validation302-51/94TransmittalNo.2000-1(10/1999)FormFDA2905a(6/92)300–1SECTION100PesticideAnalyticalManualVol.IpagedateE1Extractionwithacetone,liquid-liquidpartitioningwithpetroleumether/methylenechloride302-71/94E2Extractionwithacetone,removalofwaterwith40gHydromatri
4、x302-91/94E3Extractionwithacetone,removalofwaterwith25gHydromatrix302-121/94E4Extractionwithwater/acetone,liquid-liquidpartitioningwithpetroleumether/methylenechloride302-131/94E5Extractionwithacetone,liquid-liquidpartitioningwithacetone/methylenechloride302-1510/99E6Extractionwithwat
5、er/acetone,liquid-liquidpartitioningwithacetone/methylenechloride302-1510/99E7Extractionwithacetoneandsolidphaseextractioncartridges,liquid-liquidpartitioning302-1710/99C1Florisilcolumn(4g)cleanup,withonemethylenechlorideeluant302-191/94C2Charcoal/Celite/magnesiumoxidecolumncleanup302
6、-211/94C3Charcoal/SilanizedCelitecolumncleanup302-231/94C4C-18cartridgecleanup302-251/94C5Florisilcolumncleanup,withmixedethereluants302-271/94C6SAX/PSAcartridgecleanup302-2910/99Determination302-3110/97Confirmation302-321/94DG1GLC,100%methylsiloxane,200°C,EC302-331/94DG2GLC,100%methy
7、lsiloxane,200°C,FPD-P302-3510/97DG3GLC,100%methylsiloxane,200°C,ELCD-X302-371/94DG4GLC,100%methylsiloxane,200°C,ELCD-N302-391/94DG5GLC,100%methylsiloxane,200°␣C,N/P302-4110/97DG6GLC,100%methylsiloxane,130°C,FID302-431/94DG7GLC,100%methylsiloxane,130°C,EC302-451/94DG8GLC,100%methylsilo
8、xane,
