以聚合物胶束为模板制备纳米粒子以及酮和醇的一锅法缩合反应研究.pdf

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1、目录中文摘要··············································································……工英文摘要·················································································……工H第一章以聚合物胶束为模板制备纳米粒子·······································……11.1研究背景··············

2、··························································……11.1.1引言·····································，···········，················……11.1.2纳米粒子和超级组装结构的合成方法······························……21.1.3纳米空心球的制备·····················································

3、·……71.1.4空心球的功能和应用，···············································……n1.1.5本课题的提出·························································……131.2实验部分········································································……131.2.1原料及其纯化······················

4、······································……131.2.2实验步骤··································································……141.2.2.1PEO一b一P4VP的合成···················································……141.2.2.2以PEO一b一P4VP胶束为模板制备纳米粒子·····················……巧1.2.3测试与

5、表征·······························································……161.3结果讨论········································································……171.3.1PEO一b一P4VP及其胶束···················································……171.3.2模板聚合制备纳米粒子及超级组装体··········

6、····················……191.3.3聚合物空心球的制备和模板回收····································……221.3.4本章小结··································································……25参考文献··············································································……25第二章醇和酮的一锅

7、法缩合反应研究·············································……302.1研究背景········································································……302.1.1胶束催化和聚合物负载的催化剂····································……302.1.2CrO:氧化醇的反应和Claisen一Schmidt缩合反应···············……322.1.3

8、通过醇和酮缩合反应一锅法制备a，p一不饱和拨基化合物······……352.1.4木课题的提出·······················································……“…372.2实验部分········································································……382.2.1原料及其纯