马拉硫磷实验

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1、马拉硫磷实验马拉硫磷保温反应液：未稀释进样O.luL色谱ttRtx-1,柱温110度,5度/min到150度,20度/min到250度，保持18min0气化和检测温度：250度棕色：保温9h,蓝色12h,玫魂色14h,黑色16h,（均为44#保温反应液加入少量丙酮）绿色：二乙酯反应液48#44#保温反应液扣除丙酮峰后归一化结杲9h峰号保留时间组分名面积血枳％11.779398196.53.236522.1484349.20.035332.5629610.50.078142.6315021.00.040

2、853.167硫化物316179.52.569963.3222227.40.018173.7194634.90.037783.929二乙酯4748.20.038694.13890224.00.7333104.210111069.20.9028115.5522338.00.0190126.2088430.40.0685136.29727271.80.2217146.638263501.92.1417157.04910883.30.0885168.2353434.50.02799.0873971.70.0

3、3239.25014492.10.117811.3762273.10.018511.9425147.20.041812.4423523.00.028612.5684635.70.037713.026219178.31.781413.450232555.01.890213.716马拉硫磷10266349.883.443213.87251275.60.416814.34870933.40.576514.5183467.40.028214.59720886.80.169814.67567403.50.547

4、815.12255259.80.449117.2887600.80.061817.5122749.60.022317.5982462.30.020021.0094608.70.037521.2202504.60.0204保留时间组分名面积血枳％1.779206823.91.62932.149458230.03612.5629702.40.07642.6315256.10.04143.167硫化物337940.62.66213.7193852.40.03033.927二乙酯2078.60.01644.1

5、3676259.10.60074.20937046.60.29186.2076507.60.05136.29527784.90.21896.636238739.91.88077.0478747.00.06898.2322079.80.01649.0854205.10.03319.24914444.80.11389.8964811.70.037911.3762008.20.015811.9425670.00.044712.4472360.80.018612.5663318.00.026113.03322

6、7106.91.789013.455239882.91.889713.722马拉硫磷10928360.486.088513.87555357.50.436113.9842092.00.016514.34949444.90.389514.5284168.30.032814.59926917.40.212014.67778393.30.617515.12459511.40.468817.2883861.90.030417.5133450.30.027217.5993059.10.024121.008553

7、9.70.043621.2322972.90.0234保留时间组分名面积血枳％1.779200910.51.62992.1493731.00.03032.5629568.20.07762.6315068.10.04113.168硫化物356492.72.89213.7183434.00.02793.927二乙酯2881.90.02344.13670413.30.57124.20855855.40.45316.2074663.50.03786.29626889.60.21816.638259697.22

8、.10687.0509380.90.07619.0873809.30.03099.25017077.90.13859.8965767.90.046811.3762424.80.019711.9415274.00.042812.5653493.60.028313.030228159.71.851013.455221844.61.799713.718马拉硫磷10578980.285.822513.87352303.30.424314.34748796.10.