TOLUENE IN BLOOD NMAM 8007, ISSUE 1 BACKUP DATA REPORT

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1、TOLUENEINBLOODNMAM8007,ISSUE1BACKUPDATAREPORTLEEC.STONEJAMESB.PERKINSFINALAPRIL18,2003EDITED:MAY30,2012CONTRACTCDC-200-2001-08000SubmittedTo:NationalInstituteforOccupationalSafetyandHealthRobertA.TaftLaboratories4676ColumbiaParkwayCincinnati,Ohio45226SubmittedBy:ALSEnvironmental,former

2、lyDataChemLaboratories,Inc.960WestLeVoyDriveSaltLakeCity,Utah84123-2547TABLEOFCONTENTSTOLUENEinbloodINTRODUCTIONANDBACKGROUND.................................................................................1REAGENTSANDMATERIALS...........................................................

3、.....................................2PreparationofPrimaryStockandInternalStandardSolutions........................................5SAMPLEPREPARATIONANDINSTRUMENTCONDITIONS............................................6SamplePreparation....................................................

4、.......................................................6InstrumentConditions.......................................................................................................7OptimizationofInstrumentConditions........................................................................

5、....8Calibration.......................................................................................................................12ChromatographicConditions..........................................................................................13MATRIXEFFECTS...................

6、................................................................................................13LIMITOFDETECTIONANDQUANTITATIONSTUDY.....................................................15LONG-TERMSTABILITYSTUDY..........................................................................

7、...............16PRECISION,ACCURACY,ANDBIASSTUDY.....................................................................20SUMMARY................................................................................................................................21REFERENCES..................