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1、OrganicStructureDeterminationUsing2-DNMRSpectroscopyThispageintentionallyleftblankOrganicStructureDeterminationUsing2-DNMRSpectroscopyAProblem-BasedApproachJeffreyH.SimpsonDepartmentofChemistryInstrumentationFacilityMassachusettsInstituteofTechnology
2、Cambridge,MassachusettsAMSTERDAM•BOSTON•HEIDELBERG•LONDON•OXFORD•NEWYORKPARIS•SANDIEGO•SANFRANCISCO•SINGAPORE•SYDNEY•TOKYOAcademicPressisanimprintofElsevierAcademicPressisanimprintofElsevier30CorporateDrive,Suite400,Burlington,MA01803,USA525BStreet,S
3、uite1900,SanDiego,California92101-4495,USA84Theobald’sRoad,LondonWC1X8RR,UKThisbookisprintedonacid-freepaper.Copyright©2008,ElsevierInc.Allrightsreserved.Nopartofthispublicationmaybereproducedortransmittedinanyformorbyanymeans,electronicormechanical
4、,includingphotocopy,recording,oranyinformationstorageandretrievalsystem,withoutpermissioninwritingfromthepublisher.PermissionsmaybesoughtdirectlyfromElsevier’sScience&TechnologyRightsDepartmentinOxford,UK:phone:(44)1865843830,fax:(44)1865853333,E-m
5、ail:permissions@elsevier.com.YoumayalsocompleteyourrequestonlineviatheElsevierhomepage(http://elsevier.com),byselecting“Support&Contact”then“CopyrightandPermission”andthen“ObtainingPermissions.”LibraryofCongressCataloging-in-PublicationDataSimpson,Je
6、ffreyH.Organicstructuredeterminationusing2-DNMRspectroscopy/JeffreyH.Simpson,p.cm.Includesbibliographicalreferencesandindex.ISBN978-0-12-088522-0(pbk.:alk.paper)1.Molecularstructure.2.Organiccompounds—Analysis.3.Nuclearmagneticresonancespectroscopy.I
7、.Title.QD461.S4682008541’.22—dc222008010004BritishLibraryCataloguing-in-PublicationDataAcataloguerecordforthisbookisavailablefromtheBritishLibraryISBN:978-0-12-088522-0ForinformationonallAcademicPresspublicationsvisitourWebsiteatwww.books.elsevier.co
8、mPrintedinCanada08091011987654321DedicatedtoAlanJonesmentor,friend,andtragicherovThispageintentionallyleftblankContentsPrefacexiiiCHAPTER1Introduction11.1WhatIsNuclearMagneticResonance?11.2ConsequencesofNuclearSpin11.3ApplicationofaMagneticFieldtoaNu
