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ID:33159295
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页数:3页
时间:2019-02-21
《spectra of pure liquids:纯液体的光谱》由会员上传分享,免费在线阅读,更多相关内容在应用文档-天天文库。
1、ScienceinMotionJuniataCollegeInfraredSpectraofPlasticsPAStateStandards:1.2.11.AReadandunderstandthecentralcontentofinformationaltextsanddocumentsinallacademicareas.3.1.10.CApplypatternsasrepeatedprocessesorrecurringelementsinscienceandtechnology.3.4.10.AExplainconceptsaboutthestructureandpropertie
2、sofmatter.3.7.10.BApplyappropriateinstrumentsandapparatustoexamineavarietyofobjectsandprocesses.·Describeanddemonstratetheoperationanduseofadvancedinstrumentationinevaluatingmaterialandchemicalproperties.Introduction:Infrared(IR)lightiselectromagneticradiationwithlowerenergythanvisiblelight.Infrar
3、edlightcanmakebondsvibrate,bend,orstretch.DifferentenergiesofIRradiationarerequiredtomovebondsbasedonthebondstrengthandthemassoftheatomsinvolved.Aspecificgroupingofatomsinamolecule,orafunctionalgroup,willalwaysabsorbthesamelevelofIRenergy.Wavenumbers(inversewavelengths)areusedtomeasurethesediffere
4、ntenergiesofIRradiation.Inthisexperiment,youwillcompareinfraredspectraofplasticsamplestodeterminetheiridentities.ThisIRusesanATRaccessory.ATRstandsforattenuatedtotalreflectance.IRenergyfromalaserisreflectedoffamirror,throughthesample,thenbackdownintotheinstrument.ThisproceduremakestheIRmucheasiert
5、ouse,butitdoesreducepeaksizeconsiderably.Itwillnot,however,changethelocationofthepeaks.GuidingQuestion:Pleaseanswerthefollowingquestionbeforebeginningthelab.Willinfraredspectroscopybesufficienttopositivelyidentifyaplasticsample?Whyorwhynot?Equipment/Materials:InfraredSpectraofPlasticsRevised6/22/0
6、7Page3ScienceinMotionJuniataCollegeFTIRATRaccessoryPlasticsamplesForcepsPrinterPaperMouseMousepadKeyboard(opt.)InfraredSpectraofPlasticsRevised6/22/07Page3ScienceinMotionJuniataCollegeSafety:Alwayswearsafetyglassesinthelab.InfraredSpectraofPlasticsRevised6/22/07Page3ScienceinMotionJuniataCollegePr
7、ocedure:GettingStarted:1.TurnontheFTIRwiththeswitchatthebackleftoftheinstrument.Theinstrumentshouldwarmupforaminimumof15minutes.2.Enteranyusername.(Ex.Student)ClicktheconfigurationPlasticsorPlasticsTransmittance,
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