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1、ParticleSizeMeasurementsParticleSizeMeasurementsFundamentals,Practice,QualityHenkG.Merkus1JDrs.HenkG.MerkusFormerAss.ProfessorDelftUniversityofTechnologyParkBerkenoord302641CZPijnackerTheNetherlandsISBN:978-1-4020-9015-8e-ISBN:978-1-4020-9016-5LibraryofCongressControlNumber:2008941080©2009Springer
2、Science+BusinessMediaB.V.Nopartofthisworkmaybereproduced,storedinaretrievalsystem,ortransmittedinanyformorbyanymeans,electronic,mechanical,photocopying,microfilming,recordingorotherwise,withoutwrittenpermissionfromthePublisher,withtheexceptionofanymaterialsuppliedspecificallyforthepurposeofbeingen
3、teredandexecutedonacomputersystem,forexclusiveusebythepurchaserofthework.Printedonacid-freepaper987654321springer.comPrefaceFollowingmygraduationinphysicalorganicchemistryattheUniversityofAmster-dam,IstartedtoworkattheRoyalDutchShellLaboratoriesinAmsterdam.Myfirstassignmentwasresearchinthefieldofd
4、etergentsandindustrialchemicals.ItwasfollowedbydevelopmentworkonthermalwaxcrackingforproductionofC–C214olefinsandonacid-catalyzedsynthesisofcarboxylicacidsfromC–Colefins.36Then,Imadeasignificantchangetoanalyticalchemistry,firstatShell’sprocessdevelopmentdepartmentandlaterinthechemicalengineeringde
5、partmentofDelftUniversityofTechnology.Inbothdepartments,therewasalargevarietyofanalyti-caltechniquesanddevelopmentofnewmethodsforautomatedanalysisofsmallprocessstreams.Itwasthetimethatgaschromatographyconqueredtheworld.Inthisfield,afirmbasiswasgivenbyHenkBoer,ArieKwantesandFritsZuiderwegatShellRes
6、earchLaboratoriesinAmsterdam,bothforpackedandforcapillarycol-umns.Thepotentialofgaschromatographywashugeand,therefore,alsoinDelft,itsuseincreasedenormously.Moreover,thegrowthofthistechniquewasfacilitatedsignificantlybytherapidlydevelopingelectronicsindustry.Itnotonlyledtodigitalpeakintegratorsandp
7、ersonalcomputersbutalsoenabledcomplexmeasurementtechniques.Inaddition,Ibecameinvolvedinsurfaceareaandporositycharacteriza-tionofcatalystsandadsorbents,onwhichtopictheresearchhadbeeninitiatedbyProf.J.H.deBoer.Then