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ID：20349430
大小：662.99 KB
页数：9页
时间：2018-10-10
《gcms定量标准曲线操作》由会员上传分享，免费在线阅读，更多相关内容在工程资料-天天文库。
1、1.首先打开后处理Postrun,准样品的图谱;如下所示:GCMS定Ul:标准曲线操作IGCMSPostrunAnalysis^缺捷方式ILkb，进入后在Quantitative里打开标0j2.5TICAMICScanJ：x100,000,000)TjGCMSPostrunAnalysis(Admin)-[DataAnalysis-裹HSOlQQ>】说[ileCompoundTableViewQualitativelootsWindowKelp#1PeakLotdMethod華3Qutntit2、3、-Iff!x4、»[Scan<1►IGroupMaxIntensity:49,922,792Time19233Scan#2.069Inten.69,399,725OvenTemp26000前0714t«t0010]CITEST01团CITEST02®EITEST001®EITEST002ElTEST003NCITEST01NCITEST02samplte$t01sampltest02sam5、pltestO3samplte$tO4samplt«tO5毐鼠强01奉死蜱-noiAnalyzAdminAnalyz2005-7Acq.ttScanSampleUnknovLevel1SampleDescri5.010.012.517.520.02.020(x1,000,000)30-:10」:rc2.5MaxIntensity:49,922,792Time16.574Scan#1.750Inten.2,090,906OvenTemp235.747.510.012.515.017.520.010.0^6、7.5」5.0；2.5」0.0」一0.00007.5-5.0-▼一盞2.5-0.0-0.0017C00100gBttchTtbl*7、[^Ctlibr亀t...DataAnt...I/人Ready2.然后对目标物色谱图进行扣除背景［-］，再在EDIT下输入目标物名称，M/Z，保留时间和浓度.如下图所示：餐JgCMSPostrunAnalysis(Admin)-[DataAnalysis-塞鼠强01.QGD]FileCompoundTableWewQualitativeQuantitativeLayout8、ToolsWfindowHelp这9、B10、^lBt11、fTBjQJj12、d么13、314、follidilfid糾滿15、刮㈣边I•16、』17、汕秘IlllPdiDataExplorer2dQuantitativeProjectinTIC&MICScanProj*ctlFileName70(100.000.000)MaxIntensity:49,922792•f气Time18.311Scan#1,958Inten.'I62,461,068OvenTemp2!53.HPeak>ScanGroup7.510.012.515.018、17.520.0LoadMethodQuanti19、®EITEST003)NCITESTO1]NCITEST02jsampltestOl」《mplte$t0220、jsampltest03^sarr^ltest04Jsampltest05ffiwaoi21、O表死S$-EIO1IInten.1.0-22、0.0-11.2511.502.020JZAntlyzAdminAnaly22005-7Acq.UScanSampleUnknowLevel1Stmplt•死碑SampleDescritt1m/zAbs.Inten.2[09213258,iogH9281381Ret.Time:(11.725]-[11.808]Scantt:(1168)•[11;%BasePeak:212/350.237100-250410371D^lOO)49,922,792▲0.000Time12.129Scan#1.：11.7523、JID#MaxIntensity;49,922,7921,680,761OvenTempi91.2912.0012.25ia*eITypeIistI6<9View24、iEdit裹Ttr…1)Target*i41►25、Paxa>JsXRj^1..說DataAnt.J■A26、B2
2、3、-Iff!x4、»[Scan<1►IGroupMaxIntensity:49,922,792Time19233Scan#2.069Inten.69,399,725OvenTemp26000前0714t«t0010]CITEST01团CITEST02®EITEST001®EITEST002ElTEST003NCITEST01NCITEST02samplte$t01sampltest02sam5、pltestO3samplte$tO4samplt«tO5毐鼠强01奉死蜱-noiAnalyzAdminAnalyz2005-7Acq.ttScanSampleUnknovLevel1SampleDescri5.010.012.517.520.02.020(x1,000,000)30-:10」:rc2.5MaxIntensity:49,922,792Time16.574Scan#1.750Inten.2,090,906OvenTemp235.747.510.012.515.017.520.010.0^6、7.5」5.0；2.5」0.0」一0.00007.5-5.0-▼一盞2.5-0.0-0.0017C00100gBttchTtbl*7、[^Ctlibr亀t...DataAnt...I/人Ready2.然后对目标物色谱图进行扣除背景［-］，再在EDIT下输入目标物名称，M/Z，保留时间和浓度.如下图所示：餐JgCMSPostrunAnalysis(Admin)-[DataAnalysis-塞鼠强01.QGD]FileCompoundTableWewQualitativeQuantitativeLayout8、ToolsWfindowHelp这9、B10、^lBt11、fTBjQJj12、d么13、314、follidilfid糾滿15、刮㈣边I•16、』17、汕秘IlllPdiDataExplorer2dQuantitativeProjectinTIC&MICScanProj*ctlFileName70(100.000.000)MaxIntensity:49,922792•f气Time18.311Scan#1,958Inten.'I62,461,068OvenTemp2!53.HPeak>ScanGroup7.510.012.515.018、17.520.0LoadMethodQuanti19、®EITEST003)NCITESTO1]NCITEST02jsampltestOl」《mplte$t0220、jsampltest03^sarr^ltest04Jsampltest05ffiwaoi21、O表死S$-EIO1IInten.1.0-22、0.0-11.2511.502.020JZAntlyzAdminAnaly22005-7Acq.UScanSampleUnknowLevel1Stmplt•死碑SampleDescritt1m/zAbs.Inten.2[09213258,iogH9281381Ret.Time:(11.725]-[11.808]Scantt:(1168)•[11;%BasePeak:212/350.237100-250410371D^lOO)49,922,792▲0.000Time12.129Scan#1.：11.7523、JID#MaxIntensity;49,922,7921,680,761OvenTempi91.2912.0012.25ia*eITypeIistI6<9View24、iEdit裹Ttr…1)Target*i41►25、Paxa>JsXRj^1..說DataAnt.J■A26、B2
3、-Iff!x
4、»[Scan<1►IGroupMaxIntensity:49,922,792Time19233Scan#2.069Inten.69,399,725OvenTemp26000前0714t«t0010]CITEST01团CITEST02®EITEST001®EITEST002ElTEST003NCITEST01NCITEST02samplte$t01sampltest02sam
5、pltestO3samplte$tO4samplt«tO5毐鼠强01奉死蜱-noiAnalyzAdminAnalyz2005-7Acq.ttScanSampleUnknovLevel1SampleDescri5.010.012.517.520.02.020(x1,000,000)30-:10」:rc2.5MaxIntensity:49,922,792Time16.574Scan#1.750Inten.2,090,906OvenTemp235.747.510.012.515.017.520.010.0^
6、7.5」5.0；2.5」0.0」一0.00007.5-5.0-▼一盞2.5-0.0-0.0017C00100gBttchTtbl*
7、[^Ctlibr亀t...DataAnt...I/人Ready2.然后对目标物色谱图进行扣除背景［-］，再在EDIT下输入目标物名称，M/Z，保留时间和浓度.如下图所示：餐JgCMSPostrunAnalysis(Admin)-[DataAnalysis-塞鼠强01.QGD]FileCompoundTableWewQualitativeQuantitativeLayout
8、ToolsWfindowHelp这
9、B
10、^lBt
11、fTBjQJj
12、d么
13、3
14、follidilfid糾滿
15、刮㈣边I•
16、』
17、汕秘IlllPdiDataExplorer2dQuantitativeProjectinTIC&MICScanProj*ctlFileName70(100.000.000)MaxIntensity:49,922792•f气Time18.311Scan#1,958Inten.'I62,461,068OvenTemp2!53.HPeak>ScanGroup7.510.012.515.0
18、17.520.0LoadMethodQuanti19、®EITEST003)NCITESTO1]NCITEST02jsampltestOl」《mplte$t0220、jsampltest03^sarr^ltest04Jsampltest05ffiwaoi21、O表死S$-EIO1IInten.1.0-22、0.0-11.2511.502.020JZAntlyzAdminAnaly22005-7Acq.UScanSampleUnknowLevel1Stmplt•死碑SampleDescritt1m/zAbs.Inten.2[09213258,iogH9281381Ret.Time:(11.725]-[11.808]Scantt:(1168)•[11;%BasePeak:212/350.237100-250410371D^lOO)49,922,792▲0.000Time12.129Scan#1.：11.7523、JID#MaxIntensity;49,922,7921,680,761OvenTempi91.2912.0012.25ia*eITypeIistI6<9View24、iEdit裹Ttr…1)Target*i41►25、Paxa>JsXRj^1..說DataAnt.J■A26、B2
19、®EITEST003)NCITESTO1]NCITEST02jsampltestOl」《mplte$t02
20、jsampltest03^sarr^ltest04Jsampltest05ffiwaoi
21、O表死S$-EIO1IInten.1.0-
22、0.0-11.2511.502.020JZAntlyzAdminAnaly22005-7Acq.UScanSampleUnknowLevel1Stmplt•死碑SampleDescritt1m/zAbs.Inten.2[09213258,iogH9281381Ret.Time:(11.725]-[11.808]Scantt:(1168)•[11;%BasePeak:212/350.237100-250410371D^lOO)49,922,792▲0.000Time12.129Scan#1.：11.75
23、JID#MaxIntensity;49,922,7921,680,761OvenTempi91.2912.0012.25ia*eITypeIistI6<9View
24、iEdit裹Ttr…1)Target*i41►
25、Paxa>JsXRj^1..說DataAnt.J■A
26、B2
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