核磁化学位移.doc

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1、Proton质子multCDCl3(CD3)2CO(CD3)2SOC6D6CD3CNCD3ODD2OSolventresidual7.262.052.507.161.943.314.79H2Os1.562.843.330.402.134.87aceticacid乙酸CH3s2.101.961.911.551.961.992.08Acetone丙酮CH3s2.172.092.091.552.082.152.22Acetonitrile氰化甲烷CH3s2.102.052.071.551.962.032.

2、06Benzene苯CHs7.367.367.377.157.377.33Tert-butylalcohol叔丁醇CH3s1.281.181.111.051.161.401.24OHCs4.191.552.18Tert-butylmethylether叔丁基甲醚CCH3s1.191.131.111.071.141.151.21OCH3s3.223.133.083.043.133.203.22BHT2,6-二甲基4叔丁基苯酚ArHs6.986.966.877.056.976.92OHCs5.016.6

3、54.795.2ArCH3s2.272.222.182.242.222.21ArC(CH3)3s1.431.411.361.381.391.40Chloroform氯仿CHs7.268.028.326.157.587.90Cyclohexane环己烷CH2s1.431.431.401.401.441.451,2-dichloroethane二氯乙烷CH2s3.733.873.902.903.813.78Dichloromethane二氯甲烷CH2s5.305.635.764.275.445.49Di

4、ethylether乙醚CH3t,71.211.111.091.111.121.181.17CH2q,73.483.413.383.263.423.493.56Diglyme二甘醇二甲醚CH2m3.653.563.513.463.533.613.67CH2m3.573.473.383.343.453.583.61OCH3s3.393.283.243.113.293.353.371,2-dimethoxyethane二甲氧基乙烷CH3s3.403.283.243.123.283.353.37CH2s3

5、.553.463.433.333.453.523.60Dimethylacetamide二甲基乙酰胺CH3COs2.091.971.961.601.972.072.08NCH3s3.023.002.942.572.963.313.06NCH3s2.942.832.782.052.832.922.90Dimethylformamide二甲基甲酰胺CHs8.027.967.957.637.927.977.92CH3s2.962.942.892.362.892.993.01CH3s2.882.782.73

6、1.862.772.862.85Dimethylsulfoxide二甲亚砜CH3s2.622.522.541.682.502.652.71Dioxane二氧六环CH2s3.713.593.573.353.603.663.75Ethanol乙醇CH3t,71.251.121.060.961.121.191.17CH2q,7d3.723.573.443.343.543.603.65OHscd1.323.394.632.47Ethylacetate乙酸乙酯CH3COs2.051.971.991.651.9

7、72.012.07CH2CH3q,74.124.054.033.894.064.094.14CH2CH3t,71.261.201.170.921.201.241.24Ethylmethyketone乙基甲基酮CH3COs2.142.072.071.582.062.122.19CH2CH3q,72.462.452.431.812.432.503.18CH2CH3t,71.060.960.910.850.961.011.26Ethyleneglycol乙二醇CHse3.763.283.343.413.5

8、13.593.65“grease”fCH3m0.860.870.920.860.88CH2Brs1.261.291.361.271.29n-hexane正己烷CH3t0.880.880.860.890.890.90CH2m1.261.281.251.241.281.29HMPAg六甲基磷酰胺CH3d,9.52.652.592.532.402.572.642.61Methanol甲醇CH3sh3.493.313.163.073.283.343.34OHsch1.093.