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1、16第27卷5031571,1985—12-05.[9]Daice1.Polyesterblockcopolymercompositionandprocessforthe[2]ToyoBoseki.Polyesterblockcopolymercomposition[P].EP:preparationthereof[P].US:7196123,2007-03-27.180970,1986-05—14,[10]Toray.Elasticpolyestertubularbody[P].JP:5000465,1993-01一[3]ToyoBose
2、ki.Continuousproductionofelasticpolyesters[P].US:O8.4680345,1987-07-14.[11]Toray.Elasticpolyesterlaminate[P].JP:5116263,1993-05-14.[4]Daice1.Methodforproducingpolyesterblockcopolymers[P].US:[12]Toray.Productionofelasticpolymer[P].JP:4275326,1992-09-20090186991,2009-7-23.30
3、.[5]Daice1.Methodoftreat
4、ngpolyesterpolymerandpolyesterpolymerre_[13]Toray.Processforcontinuousproductionofelasticpolyesters[P].ducedinlow—boilingcomponentcontent[P].US:20050075464,20O5—US:5225497,1993-07-06.04-07.[14]CHENGXiao—min,LUOXiao.1ie,LIZhi—bo,eta1.ProtonNMR[6]Dai
5、ce1.Thecontinuousmanufacturingmethodofthepolyester[P].characterizationofchainstructureinbutyleneterephthalate——JP:200320634o.2003-07-22.caprolactonecopolyesters[J].Journalofpolymerscience,1999,[7]Daice1.Themanufacturingmethodofthepolyesterblockcopolymer37:3770-3777.[P].JP:
6、04553455,2000—10—11.[15]程晓敏,马德柱,罗筱烈.对苯二甲酸丁二酯一s一己内酯多嵌段[8]Daice1.Processofcontinuouslyproducingpolyesterpolymer[P].共聚物中硬链段的受限结晶[J].化学物理学报,2001,14US:7094864,2006-08-22.(2):251-255.Synthesisandcharacterizationofpolybutyleneterephthalate—co-—caprolactoneZHAOWei,,WUShui—zhu,,XUY
7、i.bin(1.EnterpriseTechnologyCenterofKingfaScientificandTechnologicalCo.Ltd.,Guangzhou510663,China;2.SchoolofMaterialsScienceandEngineering,SouthChinaUniversityofTechnology,Guangzhou510640,China)Abstract:Usingpolybutyleneterephthalate(PBT)and—caprolactone(CL)asrawmaterial,t
8、heCLring—openingpolymerizationwasinitiatedbyPBThydroxylendgroups.Thenpolyc0ndensati0nwascarriedoutatahightempera—ture,highvacuumcondition.ThePBT-CLcopolyesterwithdifferenthardsegmentcontentwasprepared.ThePBT—CLwascharacterizedbyHNMR.IRandDSC.TheresultsshowedthePBT-CLwithab
9、lockpolymerproperties.Themeltingpointofcopolyesterriseswiththeincreasingofhardsegmentcont
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