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1、电纺聚丙烯腈基碳纳米纤维的制备吴梅玉吴艺琼刘海清*福建师范大学化学与材料学院，福建省高分子材料重点实验室，福建福州350007摘要：通过静电纺丝制备了平均直径为350nm的聚丙烯腈(PAN)纳米纤维.将PAN纳米纤维分别在250,265和280℃温度下预氧化1h后，将它们在1000℃下碳化得到碳纳米纤维.通过扫描电镜、红外光谱、差示扫描量热分析和X射线粉末衍射分析对PAN纳米纤维、预氧化后的纳米纤维及碳纳米纤维的形貌、热性能和化学结构进行了表征.结果表明，PAN纤维的最佳预氧化温度为280℃.在该温度
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