吉大仪器分析书后习题答案校对.pdf

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1、•2.6(81.92mL/min)•2.9(苯：866，2.3mm；甲苯：1.06×103，1.9mm；乙苯：1.3×103，1.5mm)•2.12(A=0.057cm，B=0.703cm2·s-1，C=0.0028s；d.最佳=15.8cm·s-1；e.=35cm·s-1)•2.13(a.1000；b.2cm·s-1)•2.15(a.0.32；b.41616或a.0.26;b.64516)•2.16(b.0.67，1.57)•2.17(388.8mm)•2.19(1.25；2216，1539；2.354)•2.2

2、2(d.53.57cm或55.25mine.0.0023cm或0.0027cm)•2.23(KB=28.17，KC=30.40，KD=34.51；e.•L=67.93cm；f.L=34.33cm；g.L=67.93cm)•3.10(1.33∗10-5μg)•3.11（IA=1003.99或1006；A和B不是同系物因为45.79(或48)不是100的整数倍）•3.12（a.15.26%，47.78%，36.97%；b.17.78min）•3.13查表CS2密度0.88(Dm=1.15×10-10mg·s-1）•3.

3、14（19.38%）•3.17（环己烷Ix=688)•4.11(黄连碱54.53%，小檗碱56.15%）•4.13(Rs=3.19,Rs=4.51•或Rs1=3.26,Rs2=4.614.11(54.53%;56.15%)4.12(1.98;原答案)4.13(b.3.26,4.61)6.5(b.-0.653;c.-2.12)6.6(8.16×10-17)6.8原答案6.9(a.-0.308;c.0.513)6.10(当SCE取0.242时,0.265;0.289;50.1;49.9;当SCE取0.244时0.287

4、；0.265；46.1；53.9)7.6(b.2.23×10-7---3.05×10-7)7.8(58.7;4.95×10-4)7.10(1×10-5)7.20(0.497→0.491)8.10(46.08)8.15原答案8.16(c.5.02)8.19(1.514)8.22(4.6×10-6)8.23(17.93%;13.16%)9.3(0.57%)9.4(1.3×10-5)9.9(0.14g/L)9.10(0.23%)9.11(0.167×10-3)9.16(-0.878)9.17(2.8×1029)9.18(

5、3.2×1010)