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1、METHOD8260BVOLATILEORGANICCOMPOUNDSBYGASCHROMATOGRAPHY/MASSSPECTROMETRY(GC/MS)1.0SCOPEANDAPPLICATION1.1Method8260isusedtodeterminevolatileorganiccompoundsinavarietyofsolidwastematrices.Thismethodisapplicabletonearlyalltypesofsamples,regardlessofwatercontent,includingvariousairsamp
2、lingtrappingmedia,groundandsurfacewater,aqueoussludges,causticliquors,acidliquors,wastesolvents,oilywastes,mousses,tars,fibrouswastes,polymericemulsions,filtercakes,spentcarbons,spentcatalysts,soils,andsediments.Thefollowingcompoundscanbedeterminedbythismethod:aAppropriatePreparat
3、ionTechnique5030/DirectbCompoundCASNo.50355031503250215041Inject.Acetone67-64-1ppccndccAcetonitrile75-05-8ppcndndndcAcrolein(Propenal)107-02-8ppccndndcAcrylonitrile107-13-1ppccndccAllylalcohol107-18-6htcndndndcAllylchloride107-05-1cndndndndcBenzene71-43-2cndccccBenzylchloride100-4
4、4-7cndndndndcBis(2-chloroethyl)sulfide505-60-2ppndndndndcBromoacetone598-31-2ppndndndndcBromochloromethane74-97-5cndccccBromodichloromethane75-27-4cndcccc4-Bromofluorobenzene(surr)460-00-4cndccccBromoform75-25-2cndccccBromomethane74-83-9cndccccn-Butanol71-36-3htcndndndc2-Butanone(
5、MEK)78-93-3ppccndndct-Butylalcohol75-65-0ppcndndndcCarbondisulfide75-15-0ppndcndccCarbontetrachloride56-23-5cndccccChloralhydrate302-17-0ppndndndndcChlorobenzene108-90-7cndccccChlorobenzene-d5(IS)cndccccChlorodibromomethane124-48-1cndcndccChloroethane75-00-3cndcccc2-Chloroethanol1
6、07-07-3ppndndndndc2-Chloroethylvinylether110-75-8cndcndndcChloroform67-66-3cndccccChloromethane74-87-3cndccccChloroprene126-99-8cndndndndc3-Chloropropionitrile542-76-7Indndndndpc(continued)CD-ROM8260B-1Revision2December1996aAppropriatePreparationTechnique5030/DirectbCompoundCASNo.
7、50355031503250215041Inject.Crotonaldehyde4170-30-3ppcndndndc1,2-Dibromo-3-chloropropane96-12-8ppndndcndc1,2-Dibromoethane106-93-4cndndcndcDibromomethane74-95-3cndcccc1,2-Dichlorobenzene95-50-1cndndcndc1,3-Dichlorobenzene541-73-1cndndcndc1,4-Dichlorobenzene106-46-7cndndcndc1,4-Dich
8、lorobenzene-d4(IS)cndndcndccis-1,
