《浙江师范大学-有机化学》化学-有机化学实验（一）1

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1、《有机化学实验(一)》课程实验教学大纲—、课程概况(CourseOutline)课程名称：冇机化学实验(一)Course：ExperimentsinOrganicChemistry1课程编号：0070300058适用学生：化学及应用化学专业CourseNumber：0070300058Designedfor:ChemistryandAppliedChemistry学分：2学时：72独立设课：是Credit：2Workload:72Independentcourse：yes预修课程：无机化学实验PriorLearning:ExperimentsinInorganic

2、Chemistry二、课程简介(CourseDescriptions)有机化学实验是一门独立的基础课程，由性质实验、基本操作实验、制备实验、设计性实验四部分组成。该课程目的在于训练学牛基本操作技能，让学牛掌握简单有机化合物的合成、纯化及结构测定方法；加深学生对化学基础理论、基本知识的理解，提高观察、分析和解决实际问题的能力，培养学牛严谨的工作作风和实事求是的科学态度。Asanindependentfundamentalcourse,ExperimentsinOrganicChemistryincludesfoursections,identificationofo

3、rganiccompounds,acquisitionofbasiclaboratoryskill,preparationoforganiccompounds,anddesignoforganicexperiments・Studentsaresupposedtoacquirethebasicexperimentskillsandknowledgeforpreparation,purification,andidentificationofregularorganiccompounds・Thecoursegivesstudentsadeeperunderstandi

4、ngoffundamentalexperimentalorganicchemistryandexposesstudentstoeachtechniqueinasystematicandin-depthway.Also,ittrainsstudentswiththeproblem-solvingabilityaswellaswithstrictnessandscientificattitude.三、实验项目一览表(ExperimentList)序号No.实验名称Title每组人数NumberofStudentsineachgroup实验时数Hours实验类型验证/综

5、合/设计ExperimentalTypeCharacterization/Comprehensiveness/Designment必做/选做Compulsory/Optional1仪器及实验室安全知识介绍14验证必做CompulsoryIntroductionofInstrumentsandSaftyRulesinOrganicChemistryLaboratoryCharacterization2熔点测定DeterminationofMeltingPoint14验证Characterization必做Compulsory3蒸憾、沸点测定Distillationa

6、ndDeterminationofBoilingPoint14验证Characterization必做Compulsory4重结晶Recrystallization14验证Characterization必做Compulsory5水蒸气蒸憾SteamDistillation14验证Characterization选做Optional6折光率的测定DeterminationofRefiactiveIndex14验证Characterization选做Optional7无水乙醇的制备PreparationofAnhydrousEthanol14验证Characteri

7、zation必做Compulsory8薄层色谱Thin-LayerChromatography14验证Characterization必做Compulsory9不饱和姪的制备及其性质PreparationandPropertiesofUnsaturatedHydrocarbons14验证Characterization选做Optional10苯乙酮的制备PreparationofAcetophenone18验证Characterization选做Optional11反・1,2•二氨基环己烷的手性拆分及其旋光度的测定SeparationandDetenninatio

8、noftr