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页数:8页
时间:2019-08-31
《Zeta电位测量-ParticleSolutions软件-草稿》由会员上传分享,免费在线阅读,更多相关内容在工程资料-天天文库。
1、Zeta电位测量1、打开仪器电源,电脑电源双击桌面快捷方式界血:运行软件,最终得到如下Sal«l•■«•♦・S.9Fd«Ir^Mia<<—jMv^*2、・・・IZ3、FWW/VJXWOULV1fJU.VPJ・3>m0i3WMu4、F49WW9Iw‘F・qIAntw)HMt*窗押0WKBmau•1z;UM1(MUIMP14Wit-2awz•行・BZ>1爼XXE2*weh亠2、选择5、PALSZeta电位测量,点击New,弹出测量窗口Basi匚Layout▼ELSZetaPotentialMeasASECAbsoluteSizeExcB、点选PALSZetaPotentialMeasurement陽PALS-Sa»plcID:TEST-Bf□回丈Eil・pHConductS・tu^Titrator■ClearStveSOtd.If沁ultMoDity.RMSRe:diMiCcrrhctance;EteclhcAettSspteCortRale:R衬e6、TDfRejectIDSflrtpleKottsTme(leoxxif)7、"r"8、3、将制备好的样品(样品虽约1.3ml)装入样品池,插入干净的电极,样品液完全浸没电极片,极板间无气泡,样品池表面擦干,连接电极线,再将样品池放入仪器的样品槽内,电极接口方向向右。(注:有机相样品只能使用石英样詁池以及耐腐蚀电极)4、在测量窗口中进行参数设置IdentificationWavelengthrunCellTypeBI-SCPInstrumentParametersC、点击左边的SettingskJBI-SCPD、选择样品池类型:_普通塑料样品池BI-SCGOElectrodeA9、b10、「SVE180C普通石英样品池180uL微量样品池IdentificationInsUumentParametersCellTypeBI-SCPvElectrodeAssemblEiMeasurementParametersAdvaneedSettings-AutomabonTimeDependentTemperatureDependentbenrooKnaven★JV-InstrumentsIdentificationInstrumentParameters曰Measurement点击左边Parameters-hil.^^ScedSettingsomationTimeDepe11、ndentTemperalureDependentationTemperature25.0RunPeriod(5ManualG.设置温度0Automatic:Target1.0000e-01H、设置单次测量的循环数量,一般建议为15〜20I>AdvancedSettings建议使用默认设置re?rrInstrumentsrEquilibrationTimesecondsIdentificationInstrumentParameters三MeasurementParametersInter~cycleBela]secondsVoltage(V)AdvancedSettingsE12、lAutomationTimeDependentTemperatureDependent-TitrationSetuppHTitrationMeasurementAdditiveTitrationMeasurement-SampleParametersLiquidParticle二DataAnalysisModelG)AutoUnknownOUser5.0FrequencyQiz)@AutoUnknownOVser10.0DriveMode©SineWave0AutotrackrerrrInstrumentsK、测量次数设置Measurements3secondsWaveIde13、ntificationInsUumentParameters-MeasurementParametefsAdvaneedSettings-AutomationITimeintervalb@tweenmeasuremiO<]AppendMeasurementnumbertoSampleJ、TimeDependent设置TimeDependentM、接受测量结果名称按照次数的白动编号0、是否使川自动变温StartingTemperature(25.0seTemperatureAutomailon
2、・・・IZ3、FWW/VJXWOULV1fJU.VPJ・3>m0i3WMu4、F49WW9Iw‘F・qIAntw)HMt*窗押0WKBmau•1z;UM1(MUIMP14Wit-2awz•行・BZ>1爼XXE2*weh亠2、选择5、PALSZeta电位测量,点击New,弹出测量窗口Basi匚Layout▼ELSZetaPotentialMeasASECAbsoluteSizeExcB、点选PALSZetaPotentialMeasurement陽PALS-Sa»plcID:TEST-Bf□回丈Eil・pHConductS・tu^Titrator■ClearStveSOtd.If沁ultMoDity.RMSRe:diMiCcrrhctance;EteclhcAettSspteCortRale:R衬e6、TDfRejectIDSflrtpleKottsTme(leoxxif)7、"r"8、3、将制备好的样品(样品虽约1.3ml)装入样品池,插入干净的电极,样品液完全浸没电极片,极板间无气泡,样品池表面擦干,连接电极线,再将样品池放入仪器的样品槽内,电极接口方向向右。(注:有机相样品只能使用石英样詁池以及耐腐蚀电极)4、在测量窗口中进行参数设置IdentificationWavelengthrunCellTypeBI-SCPInstrumentParametersC、点击左边的SettingskJBI-SCPD、选择样品池类型:_普通塑料样品池BI-SCGOElectrodeA9、b10、「SVE180C普通石英样品池180uL微量样品池IdentificationInsUumentParametersCellTypeBI-SCPvElectrodeAssemblEiMeasurementParametersAdvaneedSettings-AutomabonTimeDependentTemperatureDependentbenrooKnaven★JV-InstrumentsIdentificationInstrumentParameters曰Measurement点击左边Parameters-hil.^^ScedSettingsomationTimeDepe11、ndentTemperalureDependentationTemperature25.0RunPeriod(5ManualG.设置温度0Automatic:Target1.0000e-01H、设置单次测量的循环数量,一般建议为15〜20I>AdvancedSettings建议使用默认设置re?rrInstrumentsrEquilibrationTimesecondsIdentificationInstrumentParameters三MeasurementParametersInter~cycleBela]secondsVoltage(V)AdvancedSettingsE12、lAutomationTimeDependentTemperatureDependent-TitrationSetuppHTitrationMeasurementAdditiveTitrationMeasurement-SampleParametersLiquidParticle二DataAnalysisModelG)AutoUnknownOUser5.0FrequencyQiz)@AutoUnknownOVser10.0DriveMode©SineWave0AutotrackrerrrInstrumentsK、测量次数设置Measurements3secondsWaveIde13、ntificationInsUumentParameters-MeasurementParametefsAdvaneedSettings-AutomationITimeintervalb@tweenmeasuremiO<]AppendMeasurementnumbertoSampleJ、TimeDependent设置TimeDependentM、接受测量结果名称按照次数的白动编号0、是否使川自动变温StartingTemperature(25.0seTemperatureAutomailon
3、FWW/VJXWOULV1fJU.VPJ・3>m0i3WMu
4、F49WW9Iw‘F・qIAntw)HMt*窗押0WKBmau•1z;UM1(MUIMP14Wit-2awz•行・BZ>1爼XXE2*weh亠2、选择
5、PALSZeta电位测量,点击New,弹出测量窗口Basi匚Layout▼ELSZetaPotentialMeasASECAbsoluteSizeExcB、点选PALSZetaPotentialMeasurement陽PALS-Sa»plcID:TEST-Bf□回丈Eil・pHConductS・tu^Titrator■ClearStveSOtd.If沁ultMoDity.RMSRe:diMiCcrrhctance;EteclhcAettSspteCortRale:R衬e6、TDfRejectIDSflrtpleKottsTme(leoxxif)7、"r"8、3、将制备好的样品(样品虽约1.3ml)装入样品池,插入干净的电极,样品液完全浸没电极片,极板间无气泡,样品池表面擦干,连接电极线,再将样品池放入仪器的样品槽内,电极接口方向向右。(注:有机相样品只能使用石英样詁池以及耐腐蚀电极)4、在测量窗口中进行参数设置IdentificationWavelengthrunCellTypeBI-SCPInstrumentParametersC、点击左边的SettingskJBI-SCPD、选择样品池类型:_普通塑料样品池BI-SCGOElectrodeA9、b10、「SVE180C普通石英样品池180uL微量样品池IdentificationInsUumentParametersCellTypeBI-SCPvElectrodeAssemblEiMeasurementParametersAdvaneedSettings-AutomabonTimeDependentTemperatureDependentbenrooKnaven★JV-InstrumentsIdentificationInstrumentParameters曰Measurement点击左边Parameters-hil.^^ScedSettingsomationTimeDepe11、ndentTemperalureDependentationTemperature25.0RunPeriod(5ManualG.设置温度0Automatic:Target1.0000e-01H、设置单次测量的循环数量,一般建议为15〜20I>AdvancedSettings建议使用默认设置re?rrInstrumentsrEquilibrationTimesecondsIdentificationInstrumentParameters三MeasurementParametersInter~cycleBela]secondsVoltage(V)AdvancedSettingsE12、lAutomationTimeDependentTemperatureDependent-TitrationSetuppHTitrationMeasurementAdditiveTitrationMeasurement-SampleParametersLiquidParticle二DataAnalysisModelG)AutoUnknownOUser5.0FrequencyQiz)@AutoUnknownOVser10.0DriveMode©SineWave0AutotrackrerrrInstrumentsK、测量次数设置Measurements3secondsWaveIde13、ntificationInsUumentParameters-MeasurementParametefsAdvaneedSettings-AutomationITimeintervalb@tweenmeasuremiO<]AppendMeasurementnumbertoSampleJ、TimeDependent设置TimeDependentM、接受测量结果名称按照次数的白动编号0、是否使川自动变温StartingTemperature(25.0seTemperatureAutomailon
6、TDfRejectIDSflrtpleKottsTme(leoxxif)
7、"r"
8、3、将制备好的样品(样品虽约1.3ml)装入样品池,插入干净的电极,样品液完全浸没电极片,极板间无气泡,样品池表面擦干,连接电极线,再将样品池放入仪器的样品槽内,电极接口方向向右。(注:有机相样品只能使用石英样詁池以及耐腐蚀电极)4、在测量窗口中进行参数设置IdentificationWavelengthrunCellTypeBI-SCPInstrumentParametersC、点击左边的SettingskJBI-SCPD、选择样品池类型:_普通塑料样品池BI-SCGOElectrodeA
9、b
10、「SVE180C普通石英样品池180uL微量样品池IdentificationInsUumentParametersCellTypeBI-SCPvElectrodeAssemblEiMeasurementParametersAdvaneedSettings-AutomabonTimeDependentTemperatureDependentbenrooKnaven★JV-InstrumentsIdentificationInstrumentParameters曰Measurement点击左边Parameters-hil.^^ScedSettingsomationTimeDepe
11、ndentTemperalureDependentationTemperature25.0RunPeriod(5ManualG.设置温度0Automatic:Target1.0000e-01H、设置单次测量的循环数量,一般建议为15〜20I>AdvancedSettings建议使用默认设置re?rrInstrumentsrEquilibrationTimesecondsIdentificationInstrumentParameters三MeasurementParametersInter~cycleBela]secondsVoltage(V)AdvancedSettingsE
12、lAutomationTimeDependentTemperatureDependent-TitrationSetuppHTitrationMeasurementAdditiveTitrationMeasurement-SampleParametersLiquidParticle二DataAnalysisModelG)AutoUnknownOUser5.0FrequencyQiz)@AutoUnknownOVser10.0DriveMode©SineWave0AutotrackrerrrInstrumentsK、测量次数设置Measurements3secondsWaveIde
13、ntificationInsUumentParameters-MeasurementParametefsAdvaneedSettings-AutomationITimeintervalb@tweenmeasuremiO<]AppendMeasurementnumbertoSampleJ、TimeDependent设置TimeDependentM、接受测量结果名称按照次数的白动编号0、是否使川自动变温StartingTemperature(25.0seTemperatureAutomailon
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