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1、ModernOrganicSynthesisintheLaboratoryThispageintentionallyleftblankModernOrganicSynthesisintheLaboratoryACollectionofStandardExperimentalProceduresJieJackLiChrisLimberakisDerekA.PflumPfizerGlobalResearch&Development120071OxfordUniversityPress,Inc.,publishesworksthatfurtherOxfordUniversit
2、y’sobjectiveofexcellenceinresearch,scholarship,andeducation.OxfordNewYorkAucklandCapeTownDaresSalaamHongKongKarachiKualaLumpurMadridMelbourneMexicoCityNairobiNewDelhiShanghaiTaipeiTorontoWithofficesinArgentinaAustriaBrazilChileCzechRepublicFranceGreeceGuatemalaHungaryItalyJapanPolandPor
3、tugalSingaporeSouthKoreaSwitzerlandThailandTurkeyUkraineVietnamCopyright©2007byOxfordUniversityPress,Inc.PublishedbyOxfordUniversityPress,Inc.198MadisonAvenue,NewYork,NewYork10016www.oup.comOxfordisaregisteredtrademarkofOxfordUniversityPressAllrightsreserved.Nopartofthispublicationmayb
4、ereproduced,storedinaretrievalsystem,ortransmitted,inanyformorbyanymeans,electronic,mechanical,photocopying,recording,orotherwise,withoutthepriorpermissionofOxfordUniversityPress.LibraryofCongressCataloging-in-PublicationDataLi,JieJack.Modernorganicsynthesisinthelaboratory:acollectiono
5、fstandardexperimentalprocedures/JieJackLi,ChrisLimberakis,andDerekA.Pflum.p.cm.Includesbibliographicalreferencesandindex.ISBN978-0-19-518798-4;978-0-19-518799-1(pbk.)1.Organiccompounds—Synthesis.I.Limberakis,Chris.II.Pflum,DerekA.III.Title.QD262.L472007547′.2078—dc222006036964Thematerial
6、inthistextisintendedtoprovidegeneralguidelinesandisforinformationalpurposesonly.Althoughthematerials,safetyinformation,andproceduresdescribedinthisbookaredesignedtooffercurrent,accurateandauthoritativeinformationwithrespecttothesubjectmattercovered,theinformationandtheseproceduresshoul
7、dserveonlyasastartingpointforlaboratorypractices.TheydonotpurporttospecifyminimallegalstandardsortorepresentthepolicyoftheauthorsorOxfordUniversityPress.Thisbookissoldwiththeunderstandingthatnowarranty,guarantee,orrepresentationismadebytheauthorsorOxfordUniversityPressastoaccuracyors