基于自组装的微纳结构制备及其应用

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1、万方数据Abstracthexagonalarrangeddotsandhoneycomb，werefabricatedbycombiningreactiveionetchingandelectronbeamevaporationsputteringwithmonolayercolloidalcrystal．0nthebasisofthesepatternedcatalysts，patternedcarbonnanotubearrayswithhexagonalarrangedpillarsandhoneycombwerethensynthesize

2、dbythesequentchemicalvapordeposRionmethod．Inaddition,theformationmechanismofthehexagonalarrangednanoringsduringthepatternedcatalystpreparationwasinvestigated．Chapter4：Agreenandfacilemethodbasedonsubstrate-enhancedelectrolessdepositionisdesignedforthefabricationofthree—dimension

3、al(3D)metalnanoparticle@graphenehydrogel(MNP@GHG)composites．AgalvaniccellwasconstructedbyinducingnickelfoamasthesubstrateofGHG,toenhancethedepositionofMNPsonGHGviagalvaniccellreaction．VariousMNPswithredoxpotentialhigherthanthatofNi，includingAu，Pt，PdandCu，weresuccessfullydeposit

4、edontoGHG．Theproducedgoldnanoparticles／GHGcompositeshowedgoodelectrocatalyticactivityandwasusedtofabricateanamperometricsensortowardsuricacidwithgoodsensitivity．Chapter5：Themaincontentsandthesignificanceofthispaperweresummarized．Keywords：Self-assembly；Micro／nanostructuresIV万方数据

5、目录摘要⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯。IAbstract⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯．IIIEj录⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯．V第一章绪论⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯11．1自组装技术简介⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯11．2基于水滴自组装模板(呼吸图法)构筑蜂窝状微孔膜⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯．21．2．1呼吸图法概述⋯

6、⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯．21．2．2呼吸图的成孔过程⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯一31．2．3基于呼吸图微孔膜制备不同的微纳结构⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯31．2．4呼吸图微孔膜的应用⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯．．81．3基于自组装二维胶体晶体构筑微图案⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯101．3．1二维胶体晶体模板简介⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯101．3．2微图案汇总⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯111．3．3基于二维胶体晶体构筑微图案的方法⋯⋯

7、⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯．1l1．4基于(改性)石墨烯自组装构筑三维结构⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯141．4．1石墨烯和三维石墨烯简介⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯141．4．2CMGs在溶液中的自组装⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯．151．4．3CMGs在界面上的自组装⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯．161．4．4三维石墨烯的应用⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯181．5论文选题和设计思路⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯．．20第二章呼吸图法制备高性能微孔筛⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯

8、⋯⋯⋯⋯⋯⋯⋯．212．1引言⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯⋯212．2实验部