近红外和拉曼光谱法测定蜂蜜掺假-.研究

近红外和拉曼光谱法测定蜂蜜掺假-.研究

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时间:2019-01-30

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1、张欣硕+}:学位论文目录ABSTRACTNearinfraredspectroscopyisefficientforthedetectionofreducingsugarinhoney,whichcostlittletimeandbewithhighaccuracy.Meanwhile,datapretreatmentmethods,suchasMSC,Norrissmooth,firstderivative,secondderivative.areusefultreatmenttoimprovetheaccuracyofthemodel.Thepredictionaccu

2、racyofthemodeliShigherthanthosebuiltbyoverseasresearchers.Thisarticlestudiedthetestmethodsoffructose,glucose,sucroseandmaltosebyNear.infraredspectroscopy.Theresultsshowthat,Kennard—StonemethodiSaneffectivealgorithmtodevisethecalibrationsetandthevalidationset.MonteCarlocrossvalidationwasuse

3、dtoexcludetheoutliers.Thedeterminationcoefficientsofpredictvalueandtherealvaluefructose,glucose,sucroseandmaltoseare0.945,0.927,O.90l,0.610and0.971,0.940,0.949,0.750separatelybeforeandafterexcludedtheoutlier.Itefficientlyimprovedthedatadistributionandtheaccuracyofthemodel.Themodelbuiltwith

4、NearinfraredspectroscopyaftertheWavelettransfoIllliSnosignificantchange.butitiSlesstimeconsuming.whichiS2.76sotherthan3.65sbeforetheWavelettransforill.Thehoneysamplesthatwereusedtobuildmodel,werecollectedfromteensofprovident.thegeographicandpollenofthehoneyhavesomeimpactsonthespectrum.Itis

5、widerimplicatedundercomplexconditions.Toadapttheneedoftheactualdetection,theadulterationsampleswereincludedinthemodel.Byusingthechmometricmethods,theresultspredictedbytheNearinfraredspectroscopyareaccurateandreliable.SoitiSfeasibilitytobuildarapidonlinetestingtechnologyforthequalitycontrol

6、ofhoney.ThecrossvalidationcoefficientofdeterrninationofHⅣ匝andtotalacidwere0.571and0.640separately.ThebestpredictionaccuracyoftheBPneuralnetworkisover90%inallthedifferentwaysofadulterationinhoneysamplesincludingadulteratesucrose,glucoseseparatelyandadulteratesucroseandglucosetogether.Butthe

7、BPneuralnetworkiswithpoorstability,andithadgottotallynI张欣硕I:学位论文目录differentdiscriminateresultsforthesamesetofdata.UsingRBFneuralnetworkinstead,47iterationswaschosen,andsettheMSEaSO.05,theerrorrateofvalidationsetandtestsetwerelowerthanthatofBPneuralnetwork,andt

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