bruke红外opus操作流程

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1、1、Openthepowerbehindtheinstrumentandwaitforthe“Status”lightonthepanelturnsgreen.打开仪器背后的电源，等待“Status”灯变绿。2、DoubleclicktheiconofOPUStoopenthesoftware.双击OPUS图标打开软件。3、TheLogindialogboxopens.SelectyourUserIDfromthedrop-downlist.IfyouuseOPUSforthefirsttime,theUserIDdrop-downlistinclude

2、sthetwopre-defineduserrecordsDefaultandAdministrator.Selecteitheroneofthem.EnterOPUSinthePasswordentryfield.在登录窗口从下拉列表中选出你的用户名。如果是第一次运行OPUS，用户名下拉表中Default和Administrator可任选一个。在密码字段输入OPUS，要用大写。4、WerecommendtosellectthestandardDefault.owsworkspace.ClickontheLoginbuttonandtheAboutOPU

3、Swindowopens.建议选择标准“Default.ows”工作台设置。单击登录钮，打开上面的OPUS窗口。5、ClickontheAdvancedtabintheMeasurementdialogbox.,youcanclick“Load”buttontoloadanXPMfile(etc,c:programfilesopusxpmMIR_TR.XPM).Itisalsopossibletoenterthedatapathdefinedfortheautomaticstoringofthemeasurement.Ifyouchangethi

4、spath,makesurethatitdoesexist.在Measurement对话框中点击Advanced，在这个页面中再点击“Load”读取一个测量参数文件（例如c:programfilesopusxpmMIR_TR.XPM文件）。选择自动保存的路径，改变保存路径时，必需确认该路径是否已经存在。6、SelecttheCheckSignaltabintheMeasurementdialogbox.MakesurethatyouhavecheckedtheInterferogramoptionbutton.Ifnointerferogramp

5、eakisdisplayed,youcanmovethescanregiontotheleftorrightusingthearrowbuttonstofindthepeak.Oncetheinterferogrampeakhasbeenfound,itspositionMUSTbestoredbyclickingontheSavePeakPositionbutton.在第一次测量之前，正确的干涉峰的位置必须确定并且储存下来。在Measurement对话框，点击CheckSignal，如下图所示，点击Interferogram，显示干涉图。如果没有看到干

6、涉图，可以通过移动扫描区域（ScanRange），向左或向右移动来寻找干涉峰。一旦找到干涉峰，点击SavePeakPosition将干涉峰的位置储存下来。7、TostartthebackgroundmeasurementselecttheBasictabandclickontheBackgroundSingleChannelbutton.Beforethat,makeitsurethatthereisnothinginsamplecompartment.确定样品腔内无其他物品后，进入Basic页面，点击CollectBackground按钮即可采集背景谱

7、。8、Havingmeasuredthebackgroundspectrum,placethesampleintotheopticalpath.EntertheSampleNameanddefinetheSampleFormintheBasictab.Thisinformationwillbestoredtogetherwithyourspectrum.ClickontheSampleSingleChannelbuttontostartmeasurement.TheMeasurementDialogBoxisclosedandthespectrumwin

8、dowdisplayed.Onceagain,youcanmonitorthep