资源描述：
《最新的溶剂峰的化学位移1 NMR Sh》由会员上传分享，免费在线阅读，更多相关内容在行业资料-天天文库。
1、SupportingInformationNMRChemicalShiftsofTraceImpurities:CommonLaboratorySolvents,Organics,andGasesinDeuteratedSolventsRelevanttotheOrganometallicChemist,122GregoryR.Fulmer,*AlexanderJ.M.Miller,NathanielH.Sherden,HugoE.3322Gottlieb,AbrahamNudelman,BrianM.Stoltz,JohnE.Bercaw,andKarenI.1Goldber
2、g1DepartmentofChemistry,UniversityofWashington,Box351700,Seattle,Washington98195-1700;2ArnoldandMabelBeckmanLaboratoriesofChemicalSynthesis,andCaltechCenterforCatalysisandChemicalSynthesis,DivisionofChemistryandChemicalEngineeringCaliforniaInstituteofTechnology,Pasadena,California91125;3Depa
3、rtmentofChemistry,BarIlanUniversity,RamatGan52900,Israel.CorrectionsandComments........................................................................................................S21HNMRData(TableS1).........................................................................................
4、...................S313CNMRData(TableS2)...........................................................................................................S5IndividualSolventTables–NMRDataSortedbyChemicalShift(TablesS3–S26)............S7References.....................................................
5、.............................................................................S19S1CorrectionsandCommentsInthepreparationofthismanuscript,severalerrorswerediscoveredinthe11originalpaperandarereportedherein.WhilecomparingtheHNMRspectraldata1obtainedintoluene-d8tothatinC6D6,itwasdiscoveredthatt
6、heHNMRchemicalshiftsforaceticacid(CH3),acetonitrile(CH3)andtert-butylalcohol(OH)inC6D6hadeachbeenmisreportedat1.55ppmintheoriginalpaper;thevalueshavenowbeencorrectlylistedas1.52,0.58,and0.63ppm,respectively.Theoriginalpaper'sassignmentsforBHT'sC(3,5)andC(4)inC6D6,(CD3)2CO,(CD3)2SO,CD3CN,andC
7、D3ODwerereversedandarenowcorrected.Theresonancesfor1,2-dimethoxyethane(CH2)in(CD3)2CO,siliconegrease(CH3)inCDCl3,and2-propanol(CH3)inCD3ODhavebeencorrectedandarereportedas72.47,1.04,and1.15ppm,respectively.Noothersignificantdifferenceswerediscovere
